First, one of the purposes of this thesis is to estimate the complete crosstalk effects including the package and the pads on the surface acoustic wave (SAW) substrate. A new approach based on finite-difference time-domain (FDTD) with equivalent current source method is applied. Two kinds of patterns of one-port SAW resonators with the same package structure and inter-digital transducer (IDT) design are studied. Verification with the measurement results shows that our method is able to obtain good agreement and be used to observe the influence from the SAW pattern. Second, the equivalent current source method is extended to model the excitation of human-body¡¦s electrostatic discharge (ESD) situations. The efficiencies of sacrificial electrodes are also discussed. Finally, a novel sacrificial electrode with fractal to protect SAW devices from ESD break is proposed. Comparing with traditional electrode, the simulation results show that fractal can improve the protective efficiency greatly. Finally, a novel analysis model that can be used to analyze and optimize the impedance of an RFID transponder integrated circuit (IC) which uses backscatter encoding based on simultaneously maintaining the BER of the reader and maximizing the received power of the transponder IC is proposed. The analysis method utilizes mapping from signal constellation of the backscattered signal to the Smith chart to relate the two parameters. Given the system specification and characteristics of the reader and transponder antennas, the optimum impedances of transponder IC for binary communication system can be easily designed by using this model.

Particle separation is of great interest to many biological and biomedical applications. Flow-based methods have been used to sort particles and cells. However, the main challenge with flow based particle separation systems is the need for a sheath flow for successful operation. Existence of the sheath liquid dilutes the analyte, necessitates precise flow control between sample and sheath flow, requires a complicated design to create sheath flow and separation efficiency depends on the sheath liquid composition. In addition, current gold standard active separation techniques are only capable of separation based on particle size; hence, separation cannot be achieved for same-size particles with different densities. In this dissertation, a sheathless acoustic-based microfluidic platform using surface acoustic wave for not only size-dependent but also density-dependent particle separation has been investigated. In this platform, two different functions were incorporated within a single microfluidic channel with varying the number of pressure node and position. The first function was to align particles on the center of the microfluidic channel without adding any external sheath flow. The second function was to separate particles according to their size or density. Two different size-pairs of polystyrene particles with different diameters (3 µm and 10 µm for general size-resolution, 3 µm and 5 µm for higher size-resolution) were successfully separated. Also, the separation of two 10 µm diameter, different-density particle streams (polystyrene: 1.05 g/cm3, melamine: 1.71 g/cm3) was successfully demonstrated. The effects of the input power, the flow rate, and particle concentration on the separation efficiency were investigated. A range of high separation efficiencies with 94.8-100 % for size-based separation and 87.2 - 98.9 % for density-based separation were accomplished. In this dissertation, an acoustic-based microfluidic platform using dual acoustic streaming for active mixing has also been investigated. The rapid and high efficiency mixing of a fluorescent dye solution and deionized water in a microfluidic channel was demonstrated with single acoustic excitation by one interdigital transducer (IDT) as well as dual excitation by two IDTs. The mixing efficiencies were investigated as a function of applied voltage and flow rates. The results indicate that with the same operation parameters, the mixing efficiency with dual-IDT design increased to 96.7 % from 69.8 % achievable with the traditional single-IDT design. The effect of aperture length of the IDT on mixing efficiency was also investigated. Additionally, the effects of the polydimethylsiloxane (PDMS) channel wall thickness on the insertion loss and the particle migration to the pressure node due to acoustic radiation forces induced by SAW have been investigated. The results indicate that as the PDMS channel wall thickness decreased, the SAW insertion loss is reduced as well as the velocity of the particle migration due to acoustic forces increased significantly. As an example, reducing the side wall thickness of the PDMS channel from 8 mm to 2 mm in the design results in 31.2 % decrease in the insertion loss at the resonant frequency of 13.3 MHz and 186 % increase the particle migration velocity at the resonant frequency of 13.3 MHz with input power of 27 dBm. Lastly, a novel acoustic-based method of manipulating the particles using phase-shift has been proposed and demonstrated. The location of the pressure node was adjusted simply by modulating the relative phase difference (phase-shift) between two IDTs. As a result, polystyrene particles of 5 µm diameter trapped in the pressure node were manipulated laterally across the microfluidic channel. The lateral displacements of the particles from -72.5 µm to 73.1 µm along the x-direction were accomplished by varying the phase-shift with a range of -180° to 180°. The relationship between the particle displacement and the phase-shift of SAW was obtained experimentally and shown to agree with theoretical prediction of the particle position.

Ultrasonic wave transport in strongly scattering, disordered media is investigated via analysis of the multiply-scattered transmitted field. Measurements of transverse confinement, statistics, and correlations of the intensity were performed on an aluminum mesoglass, where aluminum beads were brazed together to form a porous slab sample. Comparison of the transverse confinement measurements with the self-consistent theory of localization was used to identify and locate a mobility edge in the sample at f = 1.1011 MHz, enabling a measurement of the critical exponent nu characterizing the Anderson transition, nu ~ 1.6–2. Infinite-range C0 correlations were observed, and observed to grow dramatically near the mobility edge, along with the C2 and C3 correlations. Measurements of the multifractal exponent Delta_2 were able to confirm the link between C0 correlations and Anderson localization. Experiments using the aluminum mesoglass with ethanol-filled pores showed evidence of two nearly-independent propagating modes, one of which appears to be characterized by a strongly renormalized diffusion coefficient. The density of states and level spacing statistics were investigated using a different mesoglass, constructed by sintering glass beads percolated on a random lattice. Direct measurements of these quantities were obtained by cutting small samples of this mesoglass, allowing individual vibrational modes to be resolved. The density of states showed a plateau extending well into the expected Debye regime, and evidence of a Boson peak was observed at low frequencies. The level spacing statistics indicated that transport in the frequency ranges measured was on the diffusive side of the mobility edge, showing agreement with the predictions of the GOE from random matrix theory. The dynamics of a suspension of bubbles were investigated using phase-based Diffusing Acoustic Wave Spectroscopy, where phase correlations were found to give additional information beyond traditional field- and intensity-based correlation measurements. / October 2015

Bond rupture is an experimental methodology that is used to augment a conventional mass balance biosensor. A good point-of-care biosensor is fast, reliable, simple, cost-effective, and detects low concentrations of the target analyte. Biosensor development is a multidisciplinary field and bond rupture testing is of technical interest to many groups. The Bond rupture methodology endows a mass probe with the ability to discern bond strength. The recognition of specific bonds by mass loading is separated from erroneous non-specific binding by a probe of the force between the analyte and the transducer. Bond rupture is achieved by acoustic excitation of the point of attachment. The force is incremented gradually until rupture occurs. The advancement of bond rupture biosensors beyond the lab requires improved understanding of the mechanisms of bond rupture by base excitation, the transducers, and the supporting hardware. Bond rupture has traditionally been used in conjunction with the Quartz Crystal Microbalance (QCM). There exists, however, a variety of sensors and transducers to which the bond rupture methodology could be applied. The time, cost and experience required for comprehensive investigation of all avenues is prohibitive. To further the development of bond rupture characteristic experiments are designed and carried out on the QCM platform. Numerical simulations are constructed which model the current bond rupture approach. This work is limited to the simulation of bond rupture by base excitation. From the results of the experimental investigation a number of improvements to the bond rupture technique are proposed. Improvements are tested by simulation and the Surface Acoustic Wave (SAW) device is selected to advance the bond rupture craft. A prototype SAW bond rupture device is designed. The prototype device is manufactured and tested, confirming the principle of SAW bond rupture. Future work is required to progress the SAW bond rupture methodology before possible integration with other sensor systems. Because of this work, and the evaluation of the SAW bond rupture prototype, much is learned about the advancement of SAW device bond rupture.

Leakage and blockage of oil and gas pipeline systems, water pipelines, pipe-work of process plants and other pipe networks can cause serious environmental, health and economic problems. There are a number of non-destructive testing (NDT) methods for detecting these defects in pipeline systems such as radiographic, ultrasonic, magnetic particle inspection, pressure transient and acoustic wave methods. In this study, the acoustic wave method and a modal frequency technique, which based on a roving mass method, are used. The aim of the thesis is to employ acoustic wave propagation based methods in conjunction with stationary wavelet transform (SWT) to identify leakage and blockage in pipe systems. Moreover, the research is also aimed at using the difference of modal frequencies of fluid-filled pipes with and without defects and a roving mass, and consequently, to develop a roving mass-based defect detection method for pipelines. In the study, the acoustic finite-element analysis (AFEA) method is employed to simulate acoustic wave propagation in small and large air-filled water-filled straight pipe and pipe networks with leakage and blockage but without flow. Computational fluid dynamics (CFD) analysis was also employed to simulate acoustic wave propagation in air-and water-filled pipes with flow, leakage and blockage. In addition, AFEA was used to predict the modal frequencies of air- and water-filled pipes with leakage and blockage in the presence of a roving mass that was traversed along the axis of the pipes. Experimental testing was conducted to validate some of the numerical results. Two major experiments were performed. The first set of experiments consisted of the measurement of acoustic wave propagation in a straight air-filled pipe with leakage and blockage. The second set of experiments concerned the measurement of acoustic wave propagation in an air-filled pipe network comprising straight pipe, elbows and T-piece and flange. The AFEA and CFD analysis of fluid-filled pipe can be used to simulate the acoustic wave propagation and acoustic wave reflectometry of a fluid-filled pipe with leakage and blockage of different sizes down to a small leakage size of 1mm diameter and a blockage depth of 1.2mm in a pipe. Similarly, the AFEA method of a static fluid-filled pipe can be used to simulate acoustic wave modal frequency analysis of a fluid-filled pipe with leakage and blockage of different sizes down to a leakage of 1mm diameter and a blockage depth of 1.2mm. Moreover, the measured signal of acoustic wave propagation in an air-filled can be successfully decomposed and de-noised using the SWT method to identify and locate leakages of different sizes down to 5mm diameter, and small blockage depth of 1.2mm. Also, the SWT approximation coefficient, detail and de-noised detail coefficient curves of an air-filled pipe with leakage and blockage and a roving mass give leakage and blockage indications that can be used to identify, locate and estimate the size of leakage and blockage in a pipe.

Les ultrasons laser font partie des techniques expérimentales d'inspection en développement pour des problématiques de contrôle non destructif toujours plus exigeantes. Ces méthodes sans contact permettent dans notre cas de générer et détecter des ondes de surface se propageant sur des distances de quelques dizaines de microns.L'objectif de cette thèse est de mettre au point et tester une méthode ultrasons lasers pour l'étude d'échantillons d'aciers polycristallins. En effet ces matériaux à la base d'un ensemble de pièces manufacturées sont composés d'une multitudes de cristaux anisotropes de tailles et d'orientations variables. Parmi les paramètres physiques d'intérêt l'évaluation des constantes élastiques ainsi que la détermination de texturations sont des facteurs essentiels dans toute application CND et leur simulation numérique. Dans un premier temps, les variations de vitesses de propagation dues à l'anisotropie et aux l'orientation différentes des cristaux sont mesurées grâce au montage expérimental en surface d'échantillons d'acier austénitique. Les résultats sont exploités sous la forme de distributions statistiques de vitesses de propagation et un protocole d'inversion est proposé pour l'évaluation des constantes élastiques. Dans une seconde partie, un échantillon d'acier moulé présentant de larges macrograins est analysé pour la mise en évidence de sous-structures au sein d'un milieu biphasique.Finalement un échantillon de soudure possédant une texturation typique avec grains allongés est étudié et la présence d'une orientation préférentielle est soulignée. / Laser ultrasonics are among the most interesting experimental technics to answer the need of industrials in NDT applications. These non contact methods allow to generate and detect elastic surface wave propagating on typical distances of several tens of microns.The main objective of this thesis is to test laser ultrasonics methods for polycristalline steel study. These materials are composed of several anisotropic crystals with differents sizes and orientations. Among the essential parameters to describe such material, the determination of elastic parameters and texturations are key to good understanting and for the modelisation of material in NDT studies.In a first part, velocities variations due to elastic anisotropy and crystalline orientation of grains is assessed by measuring surface acoustic wave velocity. The experimental results are used in the form of statistical distribution of velocity combined with a numerical model to evaluate elastic parameters.Stainless casted steel is a complex material presenting large biphasic grains. They are here studied to show the presence of sub-structures.Finally, a weld sample presenting typical structuration of ellongated grains is studied to show the presence of preferential orientation.

Polypyrol (PPy) je heterocyklický vodivý polymer s chemickou strukturou založenou na existenci systému konjugovaných elektronů mezi střídajícími se jednoduchými a dvojnými vazbami. Díky svým vynikajícím vlastnostem jako je dobrá elektrická vodivost, relativně vysoká stabilita prostředí a zároveň i jednoduchost a variabilita metod jeho přípravy, přilákal tento polymer pozornost mnoha vědců z různých vědních disciplín. Cílem výzkumu v této dizertační práci byla studie senzorického chování PPy. Za tímto účelem byla ověřena účinnost nanostruktur PPy při detekci vybraných „vysoce důležitých molekul plynů“ včetně acetonu, amoniaku, etanolu, etylenu a toluenu. V této práci byl připraven PPy ve formě nanotyčinek (NRs) pomocí elektrochemické syntézy a také ve formě nanočástic (NPs) chemickou cestou. Dále byly připraveny modifikované PPy struktury, a to funkcionalizací PPy NPs katalytickými částicemi zlata (Au), stříbra (Ag) a teluridu kademnatého (CdTe). Pro charakterizaci morfologie, složení a struktury připravených materiálů bylo použito několik komplementárních analytických (mikroskopických i spektroskopických) technik. Navíc byly využity techniky jako Ramanova a rentgenová fotoelektronová spektroskopie (XPS) pro in-situ test detekce plynů, které potvrdily potenciál připraveného materiálu, tedy PPy NRs i PPy NPs, pro využití v senzorech plynů. Za účelem výroby senzoru plynů byl připravený PPy materiál integrován do dvou typů převodníkových platforem: chemorezistivní a na bázi povrchové akustické vlny v tzv. Love módu (L-SAW). Test detekce plynů pro chemorezistivní senzory s PPy NRs ukázal pouze zanedbatelnou odpověď těchto senzorů pro oxid dusičitý a amoniak z důvodu jejich komplikované architektury. Změření odzevy tvou typú chemorezistivních senzorů-nemodifikovaného i modifikovaného PPy NPs nebylo možné z dúvodu extrémně vysoké odporu v řádu G. Nicméně multivodivé L-SAW senzory založené na holých PPy NPs či PPy NPs modifikovaných Au či Ag NPs a nebo CdTe kvantovými tečkami (QDs) vykazovaly odezvu pro nízké koncentrace všech testovaných velmi důležitých molekul plynů při pokojové teplotě (RT). Obecně měly L-SAW senzory s modifikovanou citlivou vrstvou vyšší citlivost než senzory s nemodifikovanou PPy citlivou vrstvou. Účinnost L-SAW senzoru primárně závisí na pracovní frekvenci a na výběru citlivé vrstvy v aktivní oblasti senzoru. Z otestovaných typů vrstev senzoru vuči jednotlivým plynům, modifikovaná PPy NPs s Ag NPs i Au NPs se javí jako nejlepší varianta pro detekci acetonu. Připravené L-SAW senzory na bázi PPy jsou jednoduchá a cenově přijatelná zařízení s vylepšenými detekčními vlastnostmi jako je vysoká senzitivita a nízký limit detekce (LOD), což je řadí mezi potenciální kandidáty v budoucích systémech pro kontrolu kvality vzduchu, potravin a rovněž pro diagnostiku nemocí z dechu.

The theoretical part of this thesis deals with principles and characteristics of the surface acoustic wave filter. It explained the principle of magnetostriction and piezoelectric effect, which uses a filter. In the practical part in the program Comsol Multiphysics are made three simple models of SAW filter. Some modes are founded and are compared to previously known results. In the next phase of project is further studied using the parametric analysis. In the last phase of project is applied global optimization PSO at admittance characteristic from simple 2D structure. The results are compared with the commercially produced devices.

En las últimas dos décadas, han surgido diferentes tecnologías acústicas para aplicaciones biosensoras como alternativas a tecnologías de detección bien establecidas ¿acústicas o ópticas¿ como son la Microbalanza de Cuarzo (QCM, por sus siglas en inglés) y la Resonancia de Plasmón de Superficie (SPR, de sus siglas en inglés). En la primera parte de este documento se revisan dichas tecnologías alternativas para aplicaciones en medio líquido. Como resultado de esta revisión, se determina que los dispositivos de onda acústica superficial Love (LW, de sus siglas en inglés) son los más prometedores y viables para conseguir el principal objetivo de esta Tesis, que es establecer una comparativa en las mismas condiciones entre inmnosensores desarrollados con la tecnología seleccionada en esta tesis y los inmunosensores desarrollados con QCMs de Alta Frecuencia Fundamental (HFF-QCM, por sus siglas en inglés). Después de esta revisión se presenta el estado del arte de los dispositivos LW en su aplicación como biosensores, así como una discusión de las tendencias y retos actuales de este tipo de sensores. Posteriormente se reúne la información más actualizada sobre aspectos de diseño, principios de operación y modelado de estos sensores. Algunos aspectos de diseño son estudiados y probados para establecer el diseño final de los dispositivos LW. Previamente a su fabricación, también se realizan simulaciones para modelar el comportamiento del dispositivo elegido previamente a su fabricación. Posteriormente, se describe la fabricación del dispositivo así como la celda de flujo diseñada para trabajar con el dispositivo en medios líquidos. Adicionalmente, un sistema electrónico de caracterización, previamente validado para sensores QCM, se adapta para sensores LW. Como resultados, se valida el sistema electrónico para caracterizar los sensores LW fabricados y montados en la celda de flujo y, finalmente, se desarrolla un inmunosensor para la detección del pesticida carbaril que se compara con otras tecnologías inmunosensoras. / In the last two decades, different acoustic technologies for biosensors applications have emerged as promising alternatives to other better established detection technologies ¿ acoustic or optic ones- such as traditional Quartz Crystal Microbalance (QCM) and Surface Plasmon Resonance (SPR). The alternative acoustic technologies for in liquid measurements are reviewed in this manuscript. Surface Acoustic Wave (SAW) Love Mode or Love Wave (LW) sensors are determined to be the most promising and viable option to work with for achieving the main aim of this Thesis. Such aim is the development of a LW immunosensor for its comparison with the same application based on High Fundamental Frequency-QCM (HFF-QCM) sensors and under the same conditions. Consequently, the state-of-the-art of LW devices for biosensing is provided and a discussion about the current trends and future challenges of these sensors is presented. In order to start working with suitable LW devices, upto- date information regarding the design aspects, operation principles and modeling of such devices is gathered. Some design aspects are explored and tested to establish the design of the final LW device. Different simulations for modeling the chosen device behavior are carried out before its fabrication. Later, the device fabrication is described. Next, to start working with the fabricated device in liquid media, a flow cell is designed and implemented. In addition, an electronic characterization system, previously validated for QCM sensors, is adapted and tested for the fabricated LW device. As results, the adapted electronic characterization system is validated for LW devices mounted in the fabricated flow cell and, finally, a LW-based immunosensor for the determination of carbaryl pesticide was developed and compared with other immunosensor technologies. / Rocha Gaso, MI. (2013). Analysis, implementation and validation of a Love mode surface acoustic wave device for its application as sensor of biological processes in liquid media [Tesis doctoral]. Editorial Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/32492 / Alfresco

Currently, there is no equipment to measure the real-time fit of EHMR or N-95masks which are used in harsh environments. Improper fit of these EHMRs or N-95 masks exposes the personnel to hazardous environments. Surface acoustic wave (SAW) sensors have been around for few decades and are being used in various applications. In this work, real-time PM2.5 detection using passive wireless SAW sensors is presented. The design of meander antenna at 433MHz for wireless interrogation of SAW sensor using HFSS and ADS is also presented in this thesis. This works also includes the design of YZ-lithium niobate SAW sensor including COMSOL simulation.