Foi realizado um estudo comparativo da capacidade de duas variantes do método de radiografia por raios- X em detectar trincas de fadiga em juntas sobrepostas rebitadas de laminado híbrido metal-fibra Glare® de uso aeronáutico. Durante os ensaios mecânicos de fadiga sob amplitude constante de tensão, diversos corpos de prova rebitados foram periodicamente inspecionados por raios-X, em ambas as modalidades convencional e digital. Raios-X em filmes convencionais digital. Raios-X em filmes convencionais proporcionaram ótimo detalhamento de trincas nas juntas mecânicas, enquanto que as imagens geradas pela modalidade digital apresentaram qualidade muito inferior, prejudicando ou até mesmo impedindo a avaliação do grau de integridade estrutural das juntas rebitadas. / A comparison is performed on the ability of two modalities of nondestructive X-ray radiography method in detecting fatigue cracks in riveted lap joints of aeronautical grade fiber-metal laminate Glare™. During constant amplitude loading in fatigue testing riveted specimens were periodically inspected using both the conventional and digital X-ray methodology. Conventional film X-ray modality provided high quality images of growing cracks in the mechanical joints, whereas digital radiography generated faulty images, which impaired or even prevented the structural integrity assessment of the riveted joints.

Zur schnellen und sicheren Gepäckabfertigung ist eine Automatisierung der Gepäckprüfung zweckmäßig. Es wird eine mehrstufige Prüfung des Gepäcks durchgeführt. In der ersten Stufe werden vom Gepäckstück mehrere Röntgendurchstrahlungbilder angefertigt. Bei einem Teil der Gepäckstücke wird ein kritischer Bereich festgestellt, welcher mit einer zweiten Maschine genauer untersucht werden muss. Aus diesem Grund muss durch die zweite Maschine anhand nur eines weiteren Röntgendurchstrahlungsbildes erkannt werden, wo sich der kritische Bereich nach dem Transport durch das Förderband befindet. Zur Lösung dieses als Positionswiederfindung bezeichneten Problems wurde ein Verfahren entwickelt, welches auf einer Beziehung zwischen den Momenten der Grauwertverteilung des Durchstrahlungsbildes und den Momenten der Schwächungskoeffizentenverteilung des Objektes beruht. Das Verfahren wurde anhand von simulierten Beispielen getestet. / Automatic explosive detection is advantageous for fast and secure baggage control. The baggage is controlled by a multi level system. In level 1 the baggage will be inspected by a multi view x-ray radiography machine. The machine divides the baggage into secure and rejected bags and finds in the rejected bags a critical region for further inspection by a level 2 machine. For this reason the level 2 machine has to identify by only one additional x-ray view the new position of the critical region of the bag after the transport to the level 2 machine. To solve this problem a method was developed, which uses a relation between the moments of the grey-value of x-ray scan and the moments of the x-ray attenuation coefficient of the inspected object. The method was tested with simulated scans.

Foi realizado um estudo comparativo da capacidade de duas variantes do método de radiografia por raios- X em detectar trincas de fadiga em juntas sobrepostas rebitadas de laminado híbrido metal-fibra Glare® de uso aeronáutico. Durante os ensaios mecânicos de fadiga sob amplitude constante de tensão, diversos corpos de prova rebitados foram periodicamente inspecionados por raios-X, em ambas as modalidades convencional e digital. Raios-X em filmes convencionais digital. Raios-X em filmes convencionais proporcionaram ótimo detalhamento de trincas nas juntas mecânicas, enquanto que as imagens geradas pela modalidade digital apresentaram qualidade muito inferior, prejudicando ou até mesmo impedindo a avaliação do grau de integridade estrutural das juntas rebitadas. / A comparison is performed on the ability of two modalities of nondestructive X-ray radiography method in detecting fatigue cracks in riveted lap joints of aeronautical grade fiber-metal laminate Glare™. During constant amplitude loading in fatigue testing riveted specimens were periodically inspected using both the conventional and digital X-ray methodology. Conventional film X-ray modality provided high quality images of growing cracks in the mechanical joints, whereas digital radiography generated faulty images, which impaired or even prevented the structural integrity assessment of the riveted joints.

Zur schnellen und sicheren Gepäckabfertigung ist eine Automatisierung der Gepäckprüfung zweckmäßig. Es wird eine mehrstufige Prüfung des Gepäcks durchgeführt. In der ersten Stufe werden vom Gepäckstück mehrere Röntgendurchstrahlungbilder angefertigt. Bei einem Teil der Gepäckstücke wird ein kritischer Bereich festgestellt, welcher mit einer zweiten Maschine genauer untersucht werden muss. Aus diesem Grund muss durch die zweite Maschine anhand nur eines weiteren Röntgendurchstrahlungsbildes erkannt werden, wo sich der kritische Bereich nach dem Transport durch das Förderband befindet. Zur Lösung dieses als Positionswiederfindung bezeichneten Problems wurde ein Verfahren entwickelt, welches auf einer Beziehung zwischen den Momenten der Grauwertverteilung des Durchstrahlungsbildes und den Momenten der Schwächungskoeffizentenverteilung des Objektes beruht. Das Verfahren wurde anhand von simulierten Beispielen getestet. / Automatic explosive detection is advantageous for fast and secure baggage control. The baggage is controlled by a multi level system. In level 1 the baggage will be inspected by a multi view x-ray radiography machine. The machine divides the baggage into secure and rejected bags and finds in the rejected bags a critical region for further inspection by a level 2 machine. For this reason the level 2 machine has to identify by only one additional x-ray view the new position of the critical region of the bag after the transport to the level 2 machine. To solve this problem a method was developed, which uses a relation between the moments of the grey-value of x-ray scan and the moments of the x-ray attenuation coefficient of the inspected object. The method was tested with simulated scans.

Multi-phase flows of small solid particles and gas bubbles in optically opaque fluids play a key role in both mineral and metallurgical processing, which use the principle of froth flotation and bubble flotation, respectively. To gain visual insight into such particle-laden multi-phase flows, this dissertation investigates the application of radiographic techniques, employing both X-rays and neutron radiation. Lab-scale experiments are performed with model particles in liquid foams and liquid metals, focussing on the time-resolved measurement of the particles’ motion in the multi-phase flows, aiming for a sufficient contrast-to-noise ratio in the X-ray or neutron image sequences. The model experiments in this dissertation demonstrate the capabilities of X-ray and neutron radiography to image multi-phase flows in particle-laden and optically opaque fluids, especially to measure the motions of small particles with high spatial and temporal resolution. X-ray radiography enables to track custom-tailored tracer particles acting as tools for experimental investigations of flow phenomena in three-dimensional liquid foams. Both radiographic techniques supplement each other for imaging measurements of multi-phase flows with gas bubbles and solid particles in liquid metals. However, to visualise smallest model particles in liquid metal flows, neutron radiography proves to be the more promising technique compared to X-ray radiography. All in all, this dissertation contributes to paving the way for systematic radiographic measurements and further studies of particle-laden flows in optically opaque fluids.

No description available.

Nous avons étudié in situ et en temps réel la structure de grains du silicium multi-cristallin issue de la solidification dirigée en utilisant l’imagerie X synchrotron. La radiographie X permet de suivre l’évolution de l’interface solide/liquide et de caractériser sa dynamique et sa morphologie. La topographie X nous donne des informations sur la structure de grains formée, les contraintes et les défauts issus de la solidification. Nous avons montré l’importance la préparation de l’état initial de la solidification en particulier pour les expériences de reprise sur germe. L’analyse de la morphologie de l’interface solide/liquide nous a permis de caractériser la surfusion cinétique du front de solidification, de comprendre l’évolution des sillons de joints de grains et d’analyser les mécanismes de compétition de grains ainsi que de révéler l’impact des impuretés sur la structure de grains formée à l’issue de la solidification. Le phénomène de maclage a aussi été observé dans nos expériences et nous avons démontré que les macles dans le silicium multi-cristallin peuvent être des macles de croissance. Deux types de macles ont été identifiés et le phénomène de compétition de grains en présence de macles étudié. / We studied in situ and real-time the grain structure of multi-crystalline silicon from directional solidification using synchrotron X-ray imaging techniques. X-ray Radiography gives information on the evolution, dynamics and morphology of the solid/liquid interface. X- ray Topography gives more information on the grain structure, strains and defects that occur during solidification step. We showed the importance of the preparation of the initial stage of solidification in particular in the experiments where solidification is initiated from seed. The analysis of the solid/liquid interface morphology allowed us to characterize the kinetic undercooling of the solidification front, to understand the evolution of the grains boundary grooves and to analyze the mechanisms of grain competition and also to reveal the impurities impact on the grain structure formed at the end of the solidification. We also observed twinning phenomenon in our experiments and we demonstrated that twins in multi-crystalline silicon can be growth twins. Two kinds of silicon twins have been identified and the grain competition phenomenon with twins studied.

La radiographie X, synchrotron et avec une source de laboratoire, a été appliquée pour étudier des phénomènes en relation avec la solidification directionnelle d’alliages Al-Cu sous champs externes et dépendants du temps. La formation des microstructures de solidification a été analysée durant des campagnes des vols paraboliques dans le cadre du projet XRMON. Nous avons montré que les variations du niveau de gravité modifiait la couche solutale, et donc la surfusion du liquide devant l’interface solide/liquide. En particulier, l’accélération du niveau de gravité induit une transition Colonnaire-Equiaxe pour un alliage affiné. Pour un alliage non-affiné, la vitesse de croissance des dendrites varie suivant les variations du niveau de gravité durant chaque parabole. Le second volet de ma thèse concerne l'effet d'un champ magnétique permanent sur la solidification équiaxe dans un gradient de température. Nous avons établi que le couplage entre le champ magnétique et le gradient de température génère une force Thermo-Electro-Magnétique qui modifie la trajectoire des grains équiaxes au cours de leur sédimentation. L’action de cette force est bien décrite par le modèle analytique de Wang et al., moyennant des corrections associées au confinement et à la morphologie des grains. Certains effets du champ magnétique sur le liquide ont été également révélés. / X-ray radiography with synchrotron and laboratory source was applied to study phenomena related to the directional solidification of Al-Cu alloys under external fields and time-dependent. The solidification microstructures formation has been analyzed during parabolic flight campaigns in the framework of XRMON project. We have shown that the gravity level variations modified the solutal layer and then the liquid undercooling ahead of the solid/liquid interface. In particular, the acceleration of gravity level induces the Columnar-to-Equiaxed transition in a refined alloy. For a non-refined alloy, the dendrite growth velocity changes with respect to the gravity level variations during each parabola. The second part of this thesis relates to the effect of a permanent magnetic field on the equiaxed solidification in a temperature gradient. The coupling between the magnetic field and the temperature gradient generates a Thermo-Electro-Magnetic force that modifies the equiaxed grains trajectory during their sedimentation. The action of this force is well described by an analytical model proposed by Wang et al. with additional corrections associated to the wall confinement and the grain morphology. Effects of the magnetic field on the liquid have been also revealed.

Submitted by Marco Antonio Oliveira da Silva (maosilva@ipen.br) on 2016-08-26T10:42:03Z No. of bitstreams: 0 / Made available in DSpace on 2016-08-26T10:42:03Z (GMT). No. of bitstreams: 0 / Para avaliar os níveis de exposição e a dose absorvida em pacientes submetidos a exames de tomografia computadorizada, TC, é necessário calcular os índices de dose em medições com um simulador de PMMA, ou cheio de água. O simulador deve ser capaz de reproduzir as características de absorção e espalhamento do corpo ou parte do corpo humano em um campo de radiação. As grandezas específicas em TC: índice de kerma livre no ar (Ca,100), índice de kerma no ar ponderado (CW), índice de kerma no volume total (Cvol) e produto kerma no ar-comprimento (PKL) devem ser determinadas e comparadas com os níveis de referência já existentes na literatura. Neste trabalho foi desenvolvido um simulador pediátrico craniano, já que no Brasil os níveis de referência para diagnósticos (NRDs) disponíveis foram determinados baseados em um simulador padrão adulto. O simulador desenvolvido inovou em sua construção apresentando materiais que simulam a calota craniana em osso cortical (alumínio) e osso esponjoso (PVC). O seu interior foi preenchido com água destilada. As dimensões foram escolhidas de acordo com as recomendações da Organização Mundial da Saúde e do International Commission on Radiation Units, para o tamanho da cabeça de uma criança de 0 a 5 anos: 160 mm de diâmetro e 155 mm de altura. A calota craniana tem uma espessura de 4 mm e diâmetro interno de 111,9 mm. Para avaliar seu comportamento foram realizados testes em laboratórios e em feixes clínicos. Os resultados apresentaram uma atenuação de até 23% na utilização dos materiais que simulam a calota craniana evidenciando que os valores adotados para os cálculos de NRD podem estar superestimando a dose recebida por pacientes pediátricos. Percebe-se que a dose recebida em exames de crânio apresenta uma distribuição diferente por ser parcialmente atenuada e/ou retroespalhada pela calota craniana, o que não é considerado ao se utilizar o simulador constituído apenas de PMMA. / Tese (Doutorado em Tecnologia Nuclear) / IPEN/T / Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP

L’imagerie à rayons X couplée aux détecteurs résolus en énergie permet de différencier les matériaux présents et d’estimer leurs contributions respectives. Cependant, ces techniques nécessitent des images très précises. La présence du rayonnement diffusé conduit à une perte du contraste spatial et un biais dans l’imagerie radiographique ainsi que des artefacts dans la tomodensitométrie (TDM). L’objectif principal de cette thèse était de développer une approche de correction du rayonnement diffusé adaptée à l’imagerie multi-énergies. Pour réaliser cette tâche, un objectif secondaire a été défini : la conception et la validation d’un outil de simulation capable de fournir des images du diffusé résolu en énergie dans un temps raisonnable. Une fois validé, cet outil a permis d’étudier le comportement du diffusé dans le domaine spatial et énergétique. Sur la base de cette analyse du diffusé, une approche originale dite « Partial Attenuation Spectral Scatter Separation Approach » (PASSSA) adaptée à l’imagerie multi-énergies a été développée. L’évaluation de PASSSA en mode radiographique par des simulations numériques et des mesures expérimentales a révélé des résultats remarquables en termes d’amélioration du contraste d’image et de la réduction du biais induit par la présence du diffusé. De plus, des études de simulation ont permis d’évaluer la performance de l’approche développée dans la TDM, où PASSSA s’est révélée d’être très efficace pour corriger les distorsions in-duites par le rayonnement diffusé. D’autre part, l’amélioration de la performance dans le contexte de la décomposition des matériaux de base en radiographie après avoir appliqué la méthode développée a également été analysée : l’application de PASSSA se traduit par une amélioration substantielle de l’estimation des épaisseurs des matériaux de base. Finalement, sur la base des différents résultats de validation obtenus, une analyse des développements potentiels a été menée. / X-ray imaging coupled with recently emerged energy-resolved photon counting detectors provides the ability to differentiate material components and to estimate their respective thicknesses. However, such techniques require highly accurate images. The presence of scattered radiation leads to a loss of spatial contrast and, more importantly, a bias in radiographic material imaging and computed tomography (CT). Additionally, artifacts are also introduced in the case of the latter. The main aim of the present thesis was to develop a scatter correction approach adapted for multi-energy imaging. In order to achieve this task, a secondary objective was also set. Namely, the conception and validation of a simulation tool capable of providing energy-resolved scatter simulations in a reasonable time. Once validated through simulations and experimentally, this tool gave the ability to study the behavior of scattered radiation both in spatial and energy domains. Based on the conducted scatter analysis, a Partial Attenuation Spectral Scatter Separation Approach (PASSSA) adapted for multi-energy imaging was developed. The evaluation of PASSSA in radiographic mode through simulations and experiments revealed noteworthy results both in terms of image contrast improvement and scatter induced bias reduction. Additionally, simulation studies examined the performance of the developed approach in CT, where PASSSA also proved to be quite effective at correcting scatter induced distortions. Moreover, the performance improvement in the context of basis material decomposition in radiography after applying the designed method was also analyzed. It was concluded that the application of PASSSA results in a substantial improvement in basis material thickness estimation. Finally, based on the obtained simulated and experimental method evaluation results an analysis of perspective developments was also conducted.