Dans cette thèse, nous nous sommes intéressés à la mesure et à la modélisation des propriétés d'écoulements diphasiques (perméabilités relatives) dans des milieux poreux carbonatés représentatifs de la zone de transition de réservoirs pétroliers carbonatés. Notre étude expérimentale a porté sur deux roches carbonatées de même minéralogie mais de propriétés pétrophysiques différentes (unimodale et bimodale). Les fluides utilisés sont une saumure, une huile minérale pour les expériences en mouillabilité franche à l'eau et une huile brute pour les expériences en mouillabilité altérée (obtenue par macération). Durant les expériences en « écoulements permanents », la perte de charge est mesurée continûment et le champ de saturation locale est mesuré en fin d'expérience par atténuation gamma. Les principaux résultats expérimentaux de cette étude sont les suivantes :- La mouillabilité dépend de la saturation initiale en huile et donc de la hauteur de la zone de transition. Elle a une influence sur les perméabilités relatives à l'huile ET à l'eau.- L'hystérésis des perméabilités relatives à l'eau est d'autant plus prononcée que la saturation initiale en huile augmente. Une observation similaire est faite sur la courbure des perméabilités relatives à l'huile.- Les évolutions des Sorw en fonction des Soi ne vérifient pas toutes, une loi monotone de type Land. Leur évolution dépend aussi de la structure poreuse.- Les deux types de roches carbonatés présentent une altération de mouillabilité différente, la structure vacuolaire favorisant l'altération de mouillabilité. Nos données expérimentales ont été interprétées en utilisant différents modèles d'hystérésis de la littérature. Il apparait clairement des différences entre les prédictions numériques et nos données expérimentales car ces modèles ne prennent pas en compte l'évolution de la mouillabilité. Nous avons proposé un modèle de calcul des perméabilités relatives qui décrit nos données expérimentales de manière satisfaisante. / In this work, we take an interest in measuring and modeling the multiphase flow properties (relative permeabilities) in different carbonate rock types that are representative of the transition zone of carbonate reservoirs. Our experimental study focused on two different carbonate rock types, with almost the same mineralogy, but different petrophysical properties (bimodal and unimodal). The system of fluids used is composed of brine, a mineral oil (for experiments at water-wet conditions), and a crude oil (for experiments including wettability alteration after an ageing process at high temperature). During the experiments performed by the steady-state core flooding method, the pressure drop is continuously measured along the core, and the saturation profiles are obtained at the end of the flooding, by gamma ray measurements. The main results of this study are as follows:- Wettability depends on the initial oil saturation and hence the heights above the oil-water contact. It affects the oil relative permeabilities AND water relative permeabilities- The hysteresis observed on water relative permeability is even more pronounced that the initial oil saturation increases. A similar observation is made on the curvatures of the oil relative permeability.- The evolution of Sorw as function of Soi does not always follow a classical Land correlation. Their evolution also depends on the pore structure.- The two rock types exhibit different responses to wettability alteration. The vuggy structure might promote oil-wetness.Our experimental data were interpreted using different hysteretic models of the literature. We observed significant differences between the results predicted by the models and our experimental observations which are attributed mainly to the failures to take into account the change in wettability. We proposed an improved hysteresis model, which described our experimental data satisfactorily.

Les matériaux granulaires sont souvent utilisés les chaussées à faible et moyen trafic, pour la réalisation des couches d’assise, des couches de forme et de la couche de sol support. Les sollicitations dues au trafic sont les principales causes d’endommagement de ces chaussées qui conduisent à deux modes de dégradation: l’orniérage à grand rayon et la fissuration par fatigue de la couverture bitumineuse. L’influence de la non saturation et de la teneur en fines sur la capacité portante des sols granulaires joue un rôle très important sur la rigidité mécanique ainsi que l’endommagement des structures de chaussées soumises aux chargements répétés du trafic. En plus, le phénomène d’hystérésis produit par les conditions environnementales, notamment les conditions hydriques a également une influence importante sur la rigidité de ces matériaux non liés. Cependant, la méthode de dimensionnement des chaussées neuves en France ne permet pas de prendre en compte correctement l’effet de teneur en fines et l’effet de l’hystérésis hydrique. L’objectif de la thèse est d’étudier l’effet de la non-saturation, de la teneur en fines et de l’hystérésis hydrique sur le comportement mécanique des matériaux granulaires de chaussées soumis aux chargements répétés du trafic. Nous avons réalisé une campagne d’essais à différentes teneurs en eau sur deux chemins d’humidification et de séchage, avec mesure de la succion, de la résistance au cisaillement et du comportement résilient (essais triaxiaux à chargements répétés). Finalement, à l’aide de ces résultats expérimentaux, nous avons déterminé les paramètres des modèles classiques d’élasticité non linéaire. Ces modèles sont implantés dans le code de calcul aux éléments finis CAST3M pour déterminer la déflexion de chaussées souples lorsqu’elles sont soumises à des sollicitations mécaniques de trafic et des sollicitations hydriques environnementales. / Granular materials are often used in low traffic pavement structures, with unbound granular base and sub-base layers. The load due to traffic is one of the principal damage modes for these pavements. The main design criteria for these pavements are a rutting criterion for the subgrade, a fatigue criterion for the asphalt layer. The variation of the unsaturated state and the clay content in granular materials have a significant influence on their mechanical behavior. In addition, the hysteresis phenomenon produced by the environmental conditions, including water conditions also has a very important influence on the rigidity of the unbound material. Whereas, the French design method is based on linear elastic calculations. It does not take into account theinfluence of clay content of pavement materials and the influence of the hysteresis phenomenon. Then, the objective of this thesis is to study the unsaturated state, the clay content and the hysteresis phenomenon on mechanical behavior of unbound granular materials for roads subjected to traffic loading. A series of tests for different water contents on both wetting and drying paths have been carried out with matrix suction measurements, shear tests and repeated load triaxial tests for the resilient behavior. Finally, the experimental results were simulated using the nonlinear elastic model (modified Boyce model) generally used for the resilient behavior of granular soils. These models are implemented in the finite element code and calculations have been performed with CAST3M to determine the deflection of full scale pavements at different environmental conditions.

Le but de cette étude était de déterminer si le partage de petites molécules dans un système d'emballage/aliment change lorsque le polymère passe d’un état vitreux à caoutchoutique. La sorption par un polystyrène amorphe vitreux est un processus très lent. L’hystérésis observée entre les cycles de sorption et de désorption du n-hexane peut être due principalement à la variation de la vitesse à laquelle le système évolue au voisinage de la Tg et à une augmentation du volume libre dans le polymère. La sorption de vapeur de n-hexane ne modifie pas l’état physique du système, alors que celle du toluène induit un passage de l’état vitreux à caoutchoutique. Toutefois, le comportement du coefficient de partage du système toluène/PS reste inchangé lors de la transition vitreuse du système. L'effet de plastification provoquée par la sorption des composés volatils a été étudié. La sorption de certains composés volatils induit un abaissement significatif de la température de transition vitreuse du polystyrène. L'effet plastifiant du n-hexane lors de sa sorption par le PS était plus forte que celle des autres composés étudiés. Les valeurs de coefficients de partage du p-xylène et de l'éthylbenzène entre un film de polystyrène et l'éthylène glycol sont plus faibles que celles du n-hexane et du toluène à 25 °C. Finalement, malgré les modifications structurales induites par la sorption, l’énergie d’activation du coefficient de partage n’est pas significativement modifiée lors de la transition vitreuse. / The aim of this work was to find out whether the partitioning behavior of small molecules in a polymer food packaging system changes as the system traverses through its glass transition. Sorption in glassy amorphous polystyrene is a very slow process. The large hysteresis between sorption-desorption cycles of n-hexane/PS was hypothesized to be mainly due to varying rate at which the glass transition temperature was reduced and increase in system’s volume. The equilibrium sorption in glassy amorphous polystyrene at 25 °C, of n-hexane vapor did not modify the state of the system, whereas that of toluene vapor modified the system’s state significantly. The partitioning behavior of toluene/PS remained unchanged across the glass transition of the system. The plasticization effect caused by sorption was studied and revealed that it modifies the glass transition of a volatile/PS mixtures quite significantly. Such information is useful in knowing state modifications of the system as long as sorption/migration occurs, and thus assisting interpretation. The plasticizing effect of n-hexane in amorphous PS was stronger than that of three other volatiles studied. The estimated partition coefficient values of p-xylene and ethylbenzene between polystyrene film and ethylene glycol were several times lower than the experimental values of n-hexane and toluene at 25 °C. Finally, glass transition or change from glassy to rubbery states and vice-versa does not significantly modify the activation energy of sorption.

With the world’s aging power generation network, especially in Europe and the United States, life-extension of steel plant components is increasingly a critical issue, as components are exposed to high temperatures and pressures during their lifetime, potentially resulting in carbide coarsening, making them prone to creep cavitation, possibly leading to component failure. Therefore, in order to evaluate the likelihood of component failure, non-destructive testing and evaluation procedures must be developed to properly assess the level of degradation in power station steels and ensure that end-of-life conditions are not reached. Electromagnetic (EM) inspection techniques have the potential to assess the level of degradation in power station steels through in-situ measurements. This research work introduces and examines a novel approach in the development of an EM sensor system for long term use. Specifically, it focuses on employing the developed EM sensor system technology in the monitoring of microstructural variations in power generation steels (such as boiler tubes) for in-service monitoring and evaluation during maintenance periods. In this work, controlled measurement of the EM properties (differential permeability) of cylindrical samples, machined from power station pipes (P9) and tubes (T22) in different states of degradation were carried out using two different EM sensor systems. Analytical and numerical methods (Finite Elements) were employed to calculate the sensor response to the samples and EM properties inferred by fitting the models to the measured results. The results from a closed magnetic loop sensor system were also considered, where the magnetic hysteresis curves for the steel samples were measured, from which relative incremental permeability values were obtained. It was found that the incremental permeability values measured by this system were connected to the differential permeability values obtained from the induction spectroscopy. Strong correlations have been drawn between microstructural changes (quantified using Vickers hardness measurements) in heat treated samples and EM properties (incremental and differential permeability). Finally, correlations established using the lab-based closed magnetic loop system are transferred to real-world samples, such as grade 91 open pipe / tube specimens. The measurement results verify that the techniques employed for measuring the EM properties of rod samples produce similar results for the open tube samples, demonstrating the viability of application of EM methods for assessment and monitoring of open power station pipes and tubes in-situ.

Current-Controlled Pulse Width Modulated (CC-PWM) Voltage Source Inverters (VSIs) are extensively employed in high performance drives (HPD) because of the considerable advantages offered by them, such as, excellent dynamic response and inherent over-current protection, as compared to the voltage-controlled PWM (VC-PWM) VSIs. Amongst the different types of CC-PWM techniques, hysteresis current controllers offer significant simplicity in implementation. However, conventional type of hysteresis controllers (with independent comparators) suffers from some well-known drawbacks, such as, limit cycle oscillations (especially at lower speeds of operation of machine), overshoot in current error, generation of sub-harmonic components in the current, and random (non-optimum) switching of inverter voltage vectors. Common problems associated with the conventional, as well as current error space phasor based hysteresis controllers with fixed bands (boundary), are the wide variation of switching frequency in the fundamental output cycle and variation of switching frequency with the change in speed of the load motor. These problems cause increased switching losses in the inverter, non-optimum current ripple, excess harmonics in the load current and subsequent additional machine heating. A continuously varying parabolic boundary for the current error space phasor is proposed previously to get the switching frequency variation pattern of the output voltage of the hysteresis controller based PWM inverter similar to that of voltage controlled space vector PWM (VC SVPWM) based VSI. But the major problem associated with this technique is the requirement of two outer parabolas outside the current error space phasor boundary for the identification of sector change which gives rise to some switching frequency variations in one fundamental cycle and over the entire operating speed range. It also introduces 5th and 7th harmonic components in the voltage causing 5th and 7th harmonic currents in the induction motor. These harmonic currents causes 6th harmonic torque pulsations in the machine. This thesis proposes a new technique which replaces the outer parabolas and uses current errors along orthogonal axes for detecting the sector change, so that a fast and accurate detection of sector change is possible. This makes the voltage harmonic spectrum of the proposed hysteresis controller based inverter exactly matching with that of a constant switching frequency SVPWM based inverter. This technique uses the property that the current error along one of the orthogonal axis changes its direction during sector change. So the current error never goes outside the parabolic boundary as in the case of outer parabolas based sector change technique. So the proposed new technique for sector change eliminates the 5th and 7th harmonic components from the applied voltage and thus eliminates the 5th and 7th harmonic currents in the motor. So there will be no introduction of 6th harmonic torque pulsations in the motor. Using the proposed scheme for sector change and parabolic boundary for current error space phasor, simulation study was carried out using Matlab-Simulink. Simulation study showed that the switching frequency variations in a fundamental cycle and over the entire speed range of the machine upto six step mode operation is similar to that of a VC-SVPWM based VSI. The proposed hysteresis controller is experimentally verified on a 3.7 kW IM drive fed with a two-level VSI using vector control. The proposed current error space phasor based hysteresis controller providing constant switching frequency is completely implemented on the TI TMS320LF2812 DSP controller platform. The three-phase reference currents are generated depending on the frequency command and the controller is tested with drive for the entire operating speed range of the machine in forward and reverse directions. Steady state and transient results of the proposed drive are presented in this thesis. This thesis also proposes a new hysteresis controller which eliminates parabolic boundary and replaces it with a simple online computation of the boundary. In this proposed new hysteresis controller the boundary computed in the present sampling interval is used for identifying next vector to be switched. This thesis gives a detailed mathematical explanation of how the boundary is computed and how it is used for selecting vector to be switched in a sector. It also explains how the sector in which stator voltage vector is present is determined. The most important part of this proposed hysteresis controller is the estimation of stator voltages along alpha and beta axes during active and zero vector periods. Estimation of stator voltages are carried out using current errors along alpha and beta axes and steady state equivalent circuit of induction motor. Using this estimated stator voltages along alpha and beta axes, instantaneous phase voltages are computed and used for finding individual voltage vector switching times. These switching times are used for the computation of hysteresis boundary for individual vectors. So the hysteresis boundary for individual vectors are exactly calculated and used for vector change detection, making phase voltage harmonic spectrum exactly similar to that of constant switching frequency VC SVPWM inverter. Sector change detection is very simple, since we have the estimated stator voltages along alpha and beta axes to give exact position of stator voltage vector. Simulation study to verify the steady state as well as transient performance of the proposed controller based VSI fed IM drive is carried out using Simulink tool box of Matlab Simulation Software. The proposed hysteresis controller is experimentally verified on a 3.7 kW IM drive fed with a two-level VSI using vector control. The proposed current error space phasor based hysteresis controller providing constant switching frequency profile for phase voltage is implemented on the TI TMS320LF2812 DSP controller platform. The three-phase reference currents are generated depending on the frequency command and the proposed hysteresis controller is tested with drive for the entire operating speed range of the machine in forward and reverse directions. Steady state and transient results of the proposed drive are presented for different operating conditions.

Variable-speed Induction motor drives are nowadays used for various kinds of industrial processes, transportation systems, wind turbines and household appliances in the world. The majority of drives are for general purpose speed control applications where accurate speed control is not required for entire speed range. But for high dynamic drive application, very precise and fast control of induction motor drive is essential. For such applications, sophisticated and well-performing control design is a key issue. Precise and accurate torque control of the Induction Motor (IM) can only be accomplished by vector control and direct torque control. In terms of space vector theory, vector control implies that the instantaneous torque is controlled by way of the stator current vector that is orthogonal to the rotor flux vector. Precise knowledge of the rotor flux angle is therefore essential for a vector controlled IM. IMs do not allow the flux position to be easily measured, so most modern vector controlled IM drives rely on flux estimation. This means that the flux angle is derived from a flux estimator, using the dynamic model of the IM. Given that the rotor speed of the IM is measured by a mechanical shaft sensor. Flux estimation is a fairly easy task. However, vector control of IM without mechanical shaft speed sensor is of current interest in industrial environment. The driving motivations behind the development in sensorless control are lower cost, improved reliability and operating environment. In this thesis, a sensorless vector control scheme for rotor flux estimation using current error space phasor based hysteresis controller is proposed including the method for estimation of leakage inductance, Ls. For frequencies of operation less than 25 Hz, the rotor voltage and hence the rotor flux position is computed during the inverter zero voltage space vector using steady state model of IM. For above 25 Hz, active vector period and steady state model of IM is used. The whole rotor flux estimation scheme is dependent on current error space phasor and the steady state motor model, with rotor flux as a reference vector. Since no terminal voltage sensing is involved, dead time effects will not create problem in rotor flux sensing at low frequencies of operation. But appropriate device on-state drop are compensated at low frequencies (below 5 Hz) of operation to achieve a steady state operation up to less than 1 Hz. A constant switching frequency hysteresis current controller is used in inner current control loop for the PWM regulation, with smooth transition of operation to six-step mode operation. A simple Ls estimation based on current error space phasor is also proposed to nullify the deteriorating effect on rotor flux estimation. The parameter sensitivity of the control scheme to changes in the stator resistance Rs is also investigated. The drive scheme is tested up to a low frequency operation less than 1 Hz. The extensive simulation and experiment results are presented to show the proposed scheme’s good dynamic performance extending up to six-step operation. In contrast to vector control, direct torque control (DTC) method requires the knowledge of stator resistance only and thereby decreasing the associated sensitivity to parameters variation and the elimination of speed information. DTC as compared to vector control does not require co-ordinate transformation and PI controller. DTC is easy to implement because it needs only two hysteresis comparators and a lookup table for both flux and torque control. This thesis also investigates the possibilities in improvement of direct torque control scheme for high performance induction motor drive applications. Here, two schemes are proposed based on the direct torque control scheme for IM drive using 12-sided polygonal voltage space vectors for fast torque control. The torque control scheme based on DTC algorithm is proposed using 12-sided polygonal voltage space vector. The basic DTC scheme is used to control the torque. But the IM drive is open-end type. For torque control, the voltage space vectors orthogonal to stator flux vector in 12-sided polygonal space vector structure are used as hexagonal space vector based DTC scheme. The advantages achieved due to 12-sided polygonal space vector are mainly fast torque control and small torque ripple. The fast transient of torque with precise control is achieved using voltage space vector placed with a resolution of ±15. The torque ripple will be less as 6n±1 (n=odd) harmonic torque is totally eliminated from the whole range of PWM modulation. The comparative analysis of proposed 12-sided polygonal voltage space vector based DTC and conventional hexagonal space vector based DTC is also presented. Extensive simulation and experiment results are also presented to show the fast torque control at speeds of operation ranging from 5 Hz to the rated speed. The concept of 12-sided polygonal space vector based DTC is further extended for a variable speed control scheme using estimated fundamental stator voltage for sector identification. The conventional DTC scheme uses stator flux vector for identification of the sector and the switching vector are selected based on this sector information to control stator flux and torque. However, the proposed DTC scheme selects switching vectors based on the sector information of the estimated fundamental stator voltage vector and its relative position with respect to the stator flux vector. The fundamental stator voltage estimation is based on the steady state model of IM and information of synchronous frequency which is derived from computed stator flux using a low pass filter technique. The proposed DTC scheme utilizes the exact position of fundamental stator voltage vector and stator flux vector position to select optimal switching vector for fast control of torque with small variation of stator flux within hysteresis band. The present DTC scheme allows the full load torque control with fast transient response to very low speeds of operation below 5 Hz. The extensive simulation and experiment results are presented to show the fast torque control for speed of operation from zero speed to rated speed. However, the present scheme will have all the advantages of DTC scheme using stator flux vector for sector identification. All the above propositions are first simulated by MATLAB/Simulink and subsequently verified by an experimental laboratory prototype. The proposed control schemes are experimentally verified on a 3.7 kW IM drive. The control algorithms of the sensorless vector control using current error space phasor as well as DTC using 12-sided polygonal voltage space vector are completely implemented on a TI TMS320LF2812 DSP controller platform. These are some of the constituents for chapters 2, 3 and 4 in this thesis. Additionally, the first chapter also covers a brief survey on some of the recent progresses made in the field of sensorless vector control, direct torque control and current hysteresis controller. The thesis concludes with suggestion for further exploration.

La durabilité des structures en béton armé ainsi que leur durée de vie sont étroitement liées à la mise en œuvre simultanée de nombreux phénomènes physiques et chimiques. Ceux-ci sont de diverses natures mais restent, en général, fonction des propriétés hydriques des matériaux étudiés. Ainsi, la prédiction des dégradations potentielles d'un matériau cimentaire requiert l'étude du transport de l'eau liquide et des phases gazeuses à travers ce dernier, considéré comme un milieu poreux. En milieu naturel, les structures subissent des variations périodiques de l'humidité relative extérieure (HR). Cependant, la plupart des modèles de transfert hydrique préexistants dans la littérature, s'intéresse uniquement au processus de séchage. Il existe peu de modèles décrivant à la fois l'humidification et le séchage du matériau (ces deux phénomènes se produisent dans le matériau en condition naturelle d'humidité relative (HR)). Tenir compte des phénomènes d'hystérésis dans les transferts hydriques réduit à nouveau le nombre de modèles à disposition. Ainsi, cette thèse s'attache à proposer une meilleure compréhension de l'état hydrique du béton en fonction des variations d'humidité relative extérieure, sur la base d'une nouvelle campagne expérimentale et de modélisations numériques. Un soin sera apporté afin de tenir compte dans les modèles numériques des effets d'hystérésis. Dans ce travail, nous détaillerons, tout d'abord, un modèle multi-phasiques complet. Un modèle simplifié est obtenu, sur la base de considérations théoriques et de vérifications expérimentales dans le cas où la perméabilité intrinsèque à l'eau liquide reste très inférieure à la perméabilité intrinsèque au gaz. Une étude comparative des modèles d'hystérésis couramment utilisés permet d'obtenir un jeu de modèles proposant les meilleures prédictions d'isothermes de sorption d'eau et de leurs hystérésis. Par la suite, le modèle de transport simplifié est couplé avec les modèles d'hystérésis sélectionnés afin de simuler les transferts hydriques dans des bétons soumis à des cycles d'humidification-séchage. La comparaison avec des données expérimentales révèle que la prise en compte de l'hystérésis de l'isotherme de sorption d'eau ne peut pas être négligé. De plus, il est montré que les prédictions obtenues avec des modèles d'hystérésis théoriques, sont les plus cohérentes avec les résultats expérimentaux, en particulier, pour des chemins secondaires d'hystérésis. Plusieurs scénarios (conditions environnementales, bétons différents) sont également simulés. Les résultats obtenus pointent à nouveau la nécessité de tenir compte de l'hystérésis lors de la modélisation des transferts hydriques à travers des matériaux cimentaires soumis à des variations d'humidité relative. La définition d'une profondeur pour laquelle le profil hydrique du béton est modifié par les variations périodiques d'humidité relative permet de mieux comprendre comment la modélisation de la pénétration des espèces ioniques est influencée par les cycles d'humidification-séchage. Par ailleurs, notre analyse révèle qu'il est pertinent de considérer l'effet de Knudsen pour la diffusion de la vapeur afin d'améliorer la prédiction de la diffusivité apparente / The durability of reinforced concrete structures and their service life are closely related to the simultaneous occurrence of many physical and chemical phenomena. These phenomena are diverse in nature, but in common they are dependent on the moisture properties of the material. Therefore, the prediction of the potential degradation of cementitious materials requires the study of the movement of liquid-water and gas-phase transport in the material which is considered as a porous medium. In natural environment, structures are always affected by periodic variations of external relative humidity (RH). However, most moisture transport models in the literature only focus on the drying process. There are few researches considering both drying and wetting, although these conditions represent natural RH variations. Even few studies take into account hysteresis in moisture transport. Thus, this work is devoted to better understand how the moisture behaviour within cementitious materials responds to the ambient RH changes through both experimental investigations and numerical modelling. In particular, hysteretic effects will be included in numerical modelling. In this thesis, we first recalled a complicate multi-phase continuum model. By theoretical analysis and experimental verification, a simplified model can be obtained for the case of that the intrinsic permeability to liquid-water is smaller than the intrinsic permeability to gas-phase. The review of commonly-used hysteresis models enabled to conclude a set of best models for the prediction of water vapour sorption isotherms and their hysteresis. After that, the simplified model was coupled with selected hysteresis models to simulate moisture transport under drying and wetting cycles. Compared with experimental data, numerical simulations revealed that modelling with hysteretic effects can provide much better results than non-hysteresis modelling. Among different hysteresis models, results showed that the use of the conceptual hysteresis model, which presents closed form scanning loops, can provide more accuracy predictions. Further simulations for different scenarios were also performed. All comparisons and investigations enhanced the necessity of considering hysteresis to model moisture transport for varying relative humidity at the boundary. The investigation of moisture penetration depth could provide a better understanding of how deep moisture as well as ions can move into the material. Furthermore, the analysis revealed that the consideration of Knudsen effects for diffusion of vapour can improve the prediction of the apparent diffusivity

La prochaine génération de télescopes spatiaux devra repousser les limites des technologies actuelles afin d’accroitre les performances techniques et opérationnelles. Dans le cas d’observations difficiles, l'utilisation de plus grandes ouvertures des miroirs primaires est essentielle pour obtenir la résolution optique et la sensibilité requises. Toutefois, les grandes ouvertures primaires induisent un certain nombre de défis techniques tels que la masse, le volume et la raideur du miroir. La masse et le volume doivent rester acceptables par rapport au lanceur et la raideur du miroir, qui diminue avec l’augmentation du diamètre du miroir, doit être suffisante afin que les performances ne soient pas altérées par les déformations statiques et dynamiques. Pour surmonter ces limitations, des configurations de miroirs déformables comportant des éléments de contrôle actifs sont étudiées pour les futurs télescopes spatiaux. Les actionneurs piézoélectriques, qui répondent aux exigences de puissance massique et de bande passante, peuvent être utilisés comme éléments de contrôle actifs intégrés dans la structure de miroir. Toutefois, ces actionneurs montrent en fonctionnement en boucle ouverte des comportements non linéaires indésirables, comme le fluage et l'hystérésis, qui peuvent conduire à des inexactitudes indésirables et limiter les performances des systèmes. Par conséquent, pour les miroirs déformables activés par des actionneurs piézoélectriques, la compensation des non linéarités dans les actionneurs piézoélectriques est indispensable.La conception d’un miroir léger, compact et déformable à raideur adéquate est un défi très important pour les télescopes spatiaux mais n'est pas abordée dans cette thèse. Cette thèse porte sur le contrôle de surfaces de miroirs déformables actionnés par des actionneurs piézoélectriques et en particulier sur la compensation du fluage et de l'hystérésis dans les actionneurs piézoélectriques. La technologie de miroir actif étudié (avec des pieds activés, type miroir fakir) requiert un grand nombre d’actionneurs afin de tenir les exigences en termes de planéité de surface et ne permet pas un contrôle en boucle fermée de chaque actionneur (ce type de contrôle est trop exigeant en nombre de capteurs). La compensation du fluage et de l’hystérésis est donc réalisée en boucle ouverte et s’appuie sur des modèles précis des non linéarités à compenser et sur l’implémentation de modèles inverses. Un support d’étude expérimental a été élaboré au cours de la thèse afin de valider les études théoriques par des résultats expérimentaux. Il représente une partie d’un miroir de grande taille et consiste en une plaque de verre circulaire de diamètre 300mm dont la surface peut être actionnée par 7 actionneurs piézoélectriques annulaires.Les premières chapitres de la thèse concernent l’étude de la compensation en boucle ouverte du fluage et de l’hystérésis dans un seul actionneur qui est alors considéré comme un système SISO (single input – single output). Dans le dernier chapitre de la thèse, le fluage et de l’hystérésis sont compensés dans 3 actionneurs simultanément, ceux-ci formant un système MIMO (multi input – multi output). Les apports de la thèse concernent le développement de nouveaux modèles directs et inverses de fluage et d’hystérésis qui ont été validés par des expérimentations réalisées dans un contexte difficile de par la faible étendue des amplitudes de déplacement ( de l’ordre du micromètre). / The next generation of space-based observation systems will make use of larger primary mirrors to achieve higher image resolution. Large primary mirrors lead to the increase of structural flexibility and are more susceptible to distortions. Thus maintaining optical tolerances across the mirror surface becomes increasingly difficult. The techniques of active shape control may be required for spatial mirror surfaces in future space observation systems. Piezoelectric actuators are often studied as embedded elements for the active control of mirror structures due to their excellent properties. However, unwanted nonlinear effects in piezoelectric actuators, i.e., hysteresis and creep, severely limit the service performance. This thesis aims at developing openloopcontrol laws to compensate hysteresis and creep effects in piezoelectric actuators. The studies led during this thesis are applied to the shape control of spatial mirror surfaces. An experimental setup with a small-scale mirror test structure involving multiple piezoelectric actuators is first developed and is used as support for all the measurements conducted during this thesis. Then the open-loop control methodologies of creep compensation, hysteresis compensation, and simultaneous compensation of both the nonlinear effects in a single piezoelectric actuator are respectively developed. To compensate creep, a nonlinear viscoelastic model is used to portray creep, and a new inverse model of creep based on the concept of “voltage relaxation” is proposedRegarding the hysteresis compensation, the classical Preisach model is modified by adding a derivative term in parallel to describe hysteresis more accurately with relatively few measurements, and the new inverse model is constructed in the similar way. For the simultaneous compensation of the two nonlinear effects, the hysteresis is first compensated and then, the creepof the hysteresis-compensated piezoelectric actuator is attenuated by open-loop control. The methodology is first developed for a single actuator. Finally, the shape control of a mirror surface with several piezoelectric actuators is achieved by actuating the points on the mirror surface in such a way as to reach the required displacements. The mirror test structure involving multiplepiezoelectric actuators compensated in hysteresis and creep is considered as a linear system on which the superposition principle can be applied. The influence coefficients characterizing the coupling effect between the piezoelectric actuators are determined by measurements. The influence coefficient matrix is first constructed using the superposition principle, and is then inverted. By insertion of the inverse matrix in cascade with multiple piezoelectric actuators with hysteresis and creep compensation, a feed-forward control approach to actuate the multiple interesting points of the mirror surface is developed. A number of experimental results demonstrate that the developed control methodologies are effective and feasible in practice.

Cette thèse aborde la question du Changement Catégoriel dans la Perception et propose une approche Dynamique qui s’appuie sur la Théorie des Catastrophes et le modèle de la FRONCE. Dans nos travaux, nous assimilons les catégories perceptives à des attracteurs d’un système dynamique non linéaire. Si notre postulat est juste, alors, un ensemble de phénomènes non linéaires théoriquement associés doivent pouvoir être observé conjointement dans un changement catégoriel qui pourrait alors être considéré comme une transition de phase. Nous avons porté notre attention sur le phénomène d’Hystérèse, déjà abondamment exploré en perception, ainsi que sur les phénomènes de divergence et de ralentissement critique. Au travers d’une série de sept expérimentations, nous confrontons l’ensemble de ces hypothèses. Nous avons confirmé la présence de ces trois phénomènes lors d’un changement catégoriel. Les résultats montrent que l’hystérèse, la divergence et le ralentissement critique sont des phénomènes observés conjointement lors d’un changement de catégorie, mais qu’ils sont aussi quantitativement reliés, comme permettait de le prédire le modèle de la fronce issue de la théorie des catastrophes. D’une manière générale, nous avons conclu que les catégories perceptives étaient fortement similaires à des d’attracteurs et que l’étude et la modélisation des changements dans la perception devraient présenter un aspect nécessairement dynamique. / This thesis gets into the main question of Categorial Change in Perception and proposes a Dynamical approach that relies on the Catastrophes Theory and the model of the CUSP. In this work, we claim that perceptive categories are attractors in a non linear dynamics system. If we state right, we must find out several specific phenomenon theoretically linked to a phase transition in the moment of a categorial change. We bear witness for Hysteresis, which is yet widely documented in perception. Besides and in addition, we also look for divergence and critical slowing down phenomena. Along seven experimentations, we put those hypotheses to the test and achieve to attest for the occurrence of the three predicted phenomena over the categorial change. Not only results show that hysteresis, divergence and critical slowing down occur together during a categorial change but also they are quantitatively related as predicted by the catastrophe model of the cusp. More widely, we conclude, that perceptual categories might be regarded as strongly related to attractors and that survey and modeling of changes in perception shall include inevitable dynamics considerations henceforth.

L’archipel du Cap Vert constitue de 10 iles volcaniques appartient a la zone sahelienne qui s’etend de l’atlantique jusqu’a la mer rouge. Depuis, plusieurs decennies le Cap Vert est affecte par la desertification causee en grande partie par la recession climatique et l’erosion des sols. Ces facteurs, associes a la forte pression anthropique sur les ressources, a l’orographie accidentee et a des pluies tropicales parfois diluviennes, provoquent de serieuses pertes du patrimoine foncier. Cependant, depuis son Independance en 1975, le Gouvernement a mene un vaste programme d’arborisation, de restauration des terres et d’amenagement des cours d’eau. Pourtant, tres peu de recherches ont ete menees pour evaluer les actions de protection et de conservation des sols et des eaux. Par consequent, il n’existe quasiment pas de donnees sur la problematique de la degradation des terres ni de bilans. Dans le cadre de ce travail, nous avons etudie les differents facteurs qui controlent l’erosion hydrique des sols. Nous avons plus particulierement cherche a differencier les effets des activites humaines, notamment agricoles, de ceux des facteurs climatiques comme les precipitations et la generation des ecoulements. Nous avons egalement etabli les premiers bilans d’exportations de matieres en suspension et en solution dans le contexte de l’archipel du Cap Vert. L’etude a ete menee a l’echelle de trois bassins versants de l’ile de Santiago Cap-Vert. Ces trois bassins versant (Longueira, Grande et Godim) sont localises dans la partie centrale de l’ile de Santiago et representatifs des divers modes d’occupation du sol et des differents climats de l’ile. Il existe un gradient climatique entre les trois bassins versants. En effet, Longueira qui presente une superficie de 4,18 km2, une pente moyenne de 47 %, se localise dans une zone humide couverte a 69 % par une foret et une surface agricole de 17 %. Grande avec une superficie de 1,87 km2, se localise en zone sub humide pour une pente moyenne de 50 %, il est essentiellement agricole. Godim, avec une superficie de 2,0 km2, se localise en zone semi aride, il est particulierement agricole et sa pente moyenne est de 32 %. Pour ces trois bassins versants, les ecoulements de crue a l’exutoire ont ete mesures et echantillonnes de 2004 a 2009. Le bassin versant de Longueira a fait l’objet d’un suivi plus pousse, notamment en termes de frequence d’echantillonnage et de suivi des ecoulements hors crue. Sur chaque echantillon nous avons procede a la determination de la concentration des matieres en suspension ainsi qu’a l’analyse des elements majeurs. Les resultats obtenus montrent que l’erosion mecanique dans les 3 bassins versants est caracterisee par une forte variabilite spatiale et temporelle. Sur la periode 2005-2009, le bilan moyen annuel pour les bassins versants de Longueira, Grande et Godim est de : 4266, 157 et 10,1 t.km2.an-1 respectivement. La saison humide 2006 a ete la plus erosive pour l’ensemble des trois bassins versants et particulierement dans Longueira avec 2 crues exceptionnelles qui ont genere une concentration moyenne de matieres en suspension superieure a 100 g/l. En revanche, les saisons 2005 et 2008 ont ete dans l’ensemble peu erosives car les concentrations moyennes ne depasserent pas 20 g/l. Par ailleurs, il n’y a pas eu de lames d’eau ecoulees pour les saisons 2005 et 2007 pour le bassin de Godim. Sur le bassin de Longueira, l’etude des phenomenes d’hysteresis permet de caracteriser chaque crue et de montrer que l’evolution temporelle des exportations de matieres en suspension au cours de la saison est fortement influencee par les activites agricoles. En effet, la premiere crue provoque l’exportation massive des sediments disponibles et localises dans le lit du cours d’eau. En consequence, la seconde est moins exportatrice de sediments. etc / The archipelago of Cape Verde comprises 10 volcanic islands and belongs to the Sahelian zone stretching from the Atlantic to the Red Sea. Since several decades, Cape Verde is affected by desertification caused largely by climatic recession and soil erosion. These factors, coupled with high population pressure on resources, rugged topography and torrential tropical rains, cause serious losses of lands. However, since its independence in 1975, the Government conducted an extensive program of afforestation, soil and water conservation. Nevertheless very little research has been conducted to evaluate the actions of protection and conservation of soil and water. Therefore, there is no data on the problem of land degradation or budget. As part of this work, we studied the various factors that control soil erosion by water. Specifically, we sought to differentiate the effects of human activities including agriculture, those climatic factors such as rainfall and runoff generation. We also established the first mass budget of suspended and dissolved load in the context of the archipelago of Cape Verde. The study was conducted across three watersheds of the Santiago Island, Cape Verde. These three watersheds (Longueira, Grande and Godim) are located in the central part of the island and are representative of various types of land use and of the different climates of the island. There is a climatic gradient between the three watersheds. Indeed, Longueira which covers an area of 4.18 km2, an average slope of 47 % is localized in a humid zone and covered to 69 % by forest and the agricultural area is 17 %. Grande with an area of 1.87 km2, is localized in sub humid zone for an average slope of 50 %, it is mainly agricultural. Godim, with an area of 2.0 km2, is localized in semi arid, it is particularly agriculture and its average slope is 32 %. For these three watersheds, flood flows at the outlet were measured and sampled from 2004 to 2009. Watershed Longueira has been further monitoring, particularly in terms of sampling and monitoring of flood flows out. On each sample we determined the concentration of suspended sediment and we analyzed dissolved major elements. The results show that mechanical erosion in the three watersheds is characterized by high spatial and temporal variability. Over the period 2005-2009, the average annual budget for Longueira, Grande and Godim watersheds is: 4266, 157 and 10.1 t.km2.an-1 respectively. The wet season 2006 was the most erosive for all three watersheds, particularly in Longueira with 2 exceptional floods that have generated an average concentration of suspended sediment exceeding 100 g/l. In contrast, the seasons 2005 and 2008 have been generally low erosive because mean concentrations did not exceed 20 g/l. Moreover, there was no runoff for the seasons 2005 and 2007 for the watershed of Godim. In Longueira watershed, the study of hysteresis phenomena can characterize each flood and show that the temporal evolution of suspended sediment yield during the season is strongly influenced by agricultural activities. Indeed, the first flood caused the massive export of sediment available and located in the bed of the watercourse. Accordingly, the second exported less sediment. One month after the first rains, weeding activities decreased the density of vegetation cover and deconstruct the superficial soil, which again caused a very strong export of sediments during the third run off. The results of the chemical erosion in the watershed of Longueira indicate that the budget of chemical erosion rate is 45 t.km-2.an-1 with a strong temporal variability. Indeed, the wettest seasons of 2006 and 2007 are the most export of dissolved load, whereas 2005 had a low export. The use of model mixtures EMMA (End-Members Mixing Analysis) shows that the interflow and deep, feeding the streams in dissolved elements are the main factors of chemical erosion. etc