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Call number: LD2668 .T4 1984 M93 / Master of Science

A conformação em torno elétrico é um dos métodos utilizados na fabricação de peças cerâmicas, principalmente utilitários e decorações. Porém nem todas as massas cerâmicas possuem plasticidade adequada para serem torneadas. A porcelana fosfática é um desses exemplos devido à composição de 50 % de cinza de ossos bovinos, 25 % de caulim e 25 % de feldspato. Uma massa de porcelana comercial de alta temperatura, branca e com boa plasticidade foi a referência de massa propícia para se trabalhar no torno elétrico e foi feito a caracterização desse material como distribuição granulométrica, picnometria a gás, composição química por fluorescência de raio X (FRX) e difração de raio X (DRX). Os mesmos métodos de caracterização foram feitos na porcelana fosfática. O limite de Atterberg foi utilizado como técnica para medir os teores de água das massas e a reometria por squeeze flow foi o método de análise para diferenciar massas cerâmicas plásticas e não-plásticas. Testes no torno elétrico foram feitos para concluir sobre melhoria na plasticidade da porcelana fosfática através da adição de aditivo como bentonita e polímero à base de éter celulose (MHEC). Adição de 4 % de bentonita na porcelana fosfática aumentou o índice de plasticidade de Atterberg em cerca de 100 % e as curvas de squeeze flow ficaram próximos das curvas do material de referência, apresentando assim plasticidade suficiente para fabricar peças no torno elétrico. / Throwing on electric wheel is one of techniques used to forming ceramic wares as tableware and decorative. However, ceramic body needs to have enough plasticity for hands working on throwing wheel. The phosphatic porcelain composition is 50 % of bone ash, 25 % of kaolin and 25 % of feldspar and generally has low plasticity. A commercial porcelain for throwing on the electric wheel was used as default and compared with the phosphatic porcelain. Raw material characterization as particle size distribution analysis, gas pycnometry, chemical composition by x-ray fluorescence (XRF), zeta potential and x-ray diffraction (XRD) was doing to compare both porcelains. Atterberg limits were used to measure moisture content of ceramic body and rheometry was evaluated by squeeze flow technique to determine the viscosity difference between porcelain and phosphatic porcelain. Test on the throwing wheel were made to verify plasticity improvement by addition of bentonite or a polymer based on ether cellulose (MHEC). The 4 % of bentonite addition increased about 100 % the Atterberg limit and the consequent change in the squeeze flow curves demonstrate to be similar with reference and with enough plasticity to throwing on the electric wheel. Keyword: Phosphatic porcelain. Plasticity. Throwing wheel. Bentonite. Squeeze flow.

A conformação em torno elétrico é um dos métodos utilizados na fabricação de peças cerâmicas, principalmente utilitários e decorações. Porém nem todas as massas cerâmicas possuem plasticidade adequada para serem torneadas. A porcelana fosfática é um desses exemplos devido à composição de 50 % de cinza de ossos bovinos, 25 % de caulim e 25 % de feldspato. Uma massa de porcelana comercial de alta temperatura, branca e com boa plasticidade foi a referência de massa propícia para se trabalhar no torno elétrico e foi feito a caracterização desse material como distribuição granulométrica, picnometria a gás, composição química por fluorescência de raio X (FRX) e difração de raio X (DRX). Os mesmos métodos de caracterização foram feitos na porcelana fosfática. O limite de Atterberg foi utilizado como técnica para medir os teores de água das massas e a reometria por squeeze flow foi o método de análise para diferenciar massas cerâmicas plásticas e não-plásticas. Testes no torno elétrico foram feitos para concluir sobre melhoria na plasticidade da porcelana fosfática através da adição de aditivo como bentonita e polímero à base de éter celulose (MHEC). Adição de 4 % de bentonita na porcelana fosfática aumentou o índice de plasticidade de Atterberg em cerca de 100 % e as curvas de squeeze flow ficaram próximos das curvas do material de referência, apresentando assim plasticidade suficiente para fabricar peças no torno elétrico. / Throwing on electric wheel is one of techniques used to forming ceramic wares as tableware and decorative. However, ceramic body needs to have enough plasticity for hands working on throwing wheel. The phosphatic porcelain composition is 50 % of bone ash, 25 % of kaolin and 25 % of feldspar and generally has low plasticity. A commercial porcelain for throwing on the electric wheel was used as default and compared with the phosphatic porcelain. Raw material characterization as particle size distribution analysis, gas pycnometry, chemical composition by x-ray fluorescence (XRF), zeta potential and x-ray diffraction (XRD) was doing to compare both porcelains. Atterberg limits were used to measure moisture content of ceramic body and rheometry was evaluated by squeeze flow technique to determine the viscosity difference between porcelain and phosphatic porcelain. Test on the throwing wheel were made to verify plasticity improvement by addition of bentonite or a polymer based on ether cellulose (MHEC). The 4 % of bentonite addition increased about 100 % the Atterberg limit and the consequent change in the squeeze flow curves demonstrate to be similar with reference and with enough plasticity to throwing on the electric wheel. Keyword: Phosphatic porcelain. Plasticity. Throwing wheel. Bentonite. Squeeze flow.

Thesis (MSc. Agriculture (Soil Science)) -- University of Limpopo, 2014 / Phosphorus (P) runoff from agricultural sites and the subsequent loading into surface water bodies contribute to eutrophication. Environmental concerns associated with P loading in soil have motivated the need for the development of a proper tool that will allow farmers to identify agricultural areas or management practices that have the greatest potential to accelerate eutrophication. The objective of the study was to determine the spatial variability of soil test P, soil loss potential of the farm, P application rate and methods, and map P runoff risk across the field. This study was conducted in Vierfontein Boerdery in Kriel, Mpumalanga province, South Africa (longitude 29.11258833 and latitude -26.27104340). The field was under dryland cultivation and planted to yellow maize that was rotated with soybeans. Soil samples were taken at georeferenced locations in a 100 x 100 m grid for soil analysis. Spatial layers of soil P distribution, soil loss potential as well as application rate and method were created in ArcGIS software. These layers were used as input factors in a P index model to identify areas in the farm that are vulnerable to P runoff. Results indicated a variation in soil test P. Although soil test P variation was not statistically different at P≤0.05, variation had both agronomic and environmental implications. This variation could be attributed to differences in site-specific conditions and management practices. Furthermore, soil loss potential across the study site predicted by the Revised Universal Soil Loss Equation (RUSLE) showed variation with a range of 3-15 tons/ha/yr. This variation was attributed to differences in topographic variations in the study site. There is a need for best management practices that control soil erosion to minimize P runoff into water bodies. KEYWORDS: Eutrophication, Geographic Information System, Phosphorus best management practises, Phosphorus runoff index, Soil erosion, Site-specific management.

Thesis (M.Sc. Agriculture (Agronomy)) -- University of Limpopo, 2015 / Low yields in dry bean are often reported to be associated with lack of inoculation of seeds prior to planting. This also results in little fixed nitrogen contributed by the crop. Soil phosphorus (P) is another important yield limiting factor in most of the dry bean producing regions. Two field experiments were conducted to investigate the response of dry bean cultivars to inoculation and phosphorus application under dryland farming conditions during 2011/2012 and 2012/2013 growing seasons at the Syferkuil farm of University of Limpopo. The experiments were carried out as a split split-plot arrangement in randomized complete block design with four replications. Main plot factor comprised two dry bean cultivars viz, red speckled bean and small white haricot. Rhizobium phaseoli inoculation levels (inoculated and uninoculated) were assigned in the sub-plot whilst the sub-sub plot was applied with three phosphorus rates at 0, 45 and 90 kg P kg/ha. Growth parameters, phenological characteristics and yield data were collected during the course of the experiments. The results of the two experiments showed that there was no interactive effect of treatments on growth and yield parameters. However, there was a significant interactive effect of cultivar and inoculation on phenological characteristics in both growing seasons. Main effects of cultivar and inoculation significantly affected most of the parameters measured. Inoculated red speckled bean produced tallest plants which reached 50% flowering and maturity earlier than the small white haricot variety. In both growing seasons grain yield was significantly different between the two cultivars (P ≤ 0.01). The red speckled bean produced higher grain yield of 1657 kg ha-1 and 2547 kg ha-1 in 2011/2012 and 2012/2013, respectively. In contrast, the small white haricot bean achieved grain yield of 1396 kg/ha and 1797 kg/ha in the respective seasons. Grain yield was significantly increased by approximately 16.15% and 27.50% with Rhizobium inoculation in the respective seasons. Phosphorus application at varying rates did not have a significant influence on all parameters measured the experiment in both 2011/2012 and 2012/2013 seasons.

Grain corn (Zea mays L.) production occupies more farmland than any other annual crop in Quebec and is expanding demand from the livestock sector and the emerging bioethanol industry. Corn production requires high nutrient inputs and intensive tillage (IT). Many producers have thus switched to conservation tillage systems like ridge-tillage (RT) to overcome soil compaction and erosion problems that are common in IT systems. However, fertilizer guidelines developed for IT soils are used in RT although RT adoption greatly modifies phosphorus (P) dynamics. Lower fertilizer P requirements are expected because arbuscular mycorrhizal (AM) symbiosis known to enhance plant P nutrition are minimally disrupted under RT, compared to IT systems. A two-year study was conducted on a commercial farm in the Monteregie region (Quebec, Canada) to investigate the effects of P fertilizer rates and soil P-saturation status on corn early growth, nutrition and yield. Surface soil plant-available P was monitored in situ with anionic exchange membranes (P AEM) from seeding to the end of July. The effects of indigenous AM fungi on corn parameters and rhizosphere soil P pools were also investigated in untreated (AMNI) or AM-inhibited fungicide-treated (AMI) soils. Quebec's P fertilizer guidelines underestimated the soil P fertility in studied soils. Adding inorganic P (Pi) did not improve the early corn P nutrition, growth or yield, and had little impact soil PAEM. Variations in PAEM were better explained by climatic variables. AMNI corn had similar early development and high yield, regardless of whether P fertilizer was applied, whereas AMI plants needed P fertilizer to produce optimal yield. AMNI corn had reduced dependence on Pi inputs due to more efficient uptake of soil solution P i in surface and rhizosphere soils during the first 22 days after seeding (DAS), In the rhizosphere, available-Pi pool appeared to be used first to replenish the resin-P pool, but over the longer term, AM symbiosis also enhanced NaHCO3-Po mobilization through a mechanism that remains unclear. Deeper understanding of the mechanisms by which AM fungi alter soil P dynamics will contribute to the development of more sustainable P fertilizer programs for RT systems.

Darbo tikslas – nustatyti fosforo trąšų įtaką dirvožemio elektrocheminių parametrų kaitai bei miežių grūdų kokybės parametrams. Darbo uždaviniai: o nustatyti sertifikuotų ekologiškų fosoforo trąšų fosforitmilčių įtaką dirvožemio elektrocheminėms savybėms; o nustatyti sertifikuotų fosforo trąšų įtaką žemės ūkio augalų grūdų elektrocheminėms savybėms. Darbo objektas – Lietuvos žemės ūkio universiteto Agroekologijos centro ekologinės gamybos ūkio dirvožemis bei jame auginti vasariniai miežiai. Darbo rezultatai. Lietuvos žemės ūkio universiteto Agroekologijos centro ekologinės gamybos ūkyje atlikus sertifikuotų fosforo trąšų įtakos dirvožemio elektrocheminėms savybėms tyrimus, nustatyta, kad patręšus P60 fosforitmičių norma esminiai padidėjo dirvožemio pH rodiklio reikšmė, lyginant su netręštu dirvožemiu bei tręšimu P90 ir P120 normomis. Tiriant dirvožemio savitojo elektrinio laidžio reikšmes prieš tręšimą fosforo trąšomis pavasarį ir po vasarinių miežių derliaus nuėmimo, nustatyta, kad dirvožemio savitojo elektrinio laidžio reikšmės sumažėjo esminiai. Ištyrus dirvožemio savitąjį elektrinį laidį rudenį po tręšimo fosforo trąšomis, nustatyta, kad dirvožemio savitasis elektrinis laidis esminiai padidėjo, lyginant su dirvožemio ėminiais, paimtais po vasarinių miežių nupjovimo, bet negauta esminių skirtumų, lyginant su dirvožemio ėminiais paimtais pavasarį prieš vasarinių miežių tręšimą. Patręšus didžiausia tirta P120 fosforo trąšų norma, esminiai padidėjo dirvožemio redokso... [toliau žr. visą tekstą] / The thesis aims at defining the effect of phosphatic fertilizers on the change of electrochemical parameters of the soil and the quality parameters of barleycorn. The goals of the thesis are as follows: • determination of the effect of bone meal as a certified organic phosphatic fertilizer on the electrochemical parameters of the soil. • determination of the effect of certified phosphatic fertilizers on the electrochemical parameters of the crop grain. The soil of the organic farm of the Agro-ecological Centre of the Lithuanian University of Agriculture and spring barley grown therein constitute fall within the scope of the thesis. Findings. Research of the effect of certified phosphatic fertilizers on the electrochemical parameters of the soil in the organic farm of the Agro-ecological Centre of the Lithuanian University of Agriculture shows that application of the standard P60 bone meal resulted in a considerable increase of the pH value of the soil, as compared to unfertilized soil or use of the standard P90 and P120. The analysis of the values of soil conductivity before application of phosphatic fertilizers in spring and after reaping of spring barley reveals that the values of soil conductivity decreased to a remarkable extent. After testing of soil conductivity in autumn after use of phosphatic fertilizers it was established that soil conductivity, as compared to the soil samples taken after reaping of spring barley, considerably increased, however, testing shows no... [to full text]