Les matériaux ferroélectriques suscitent beaucoup d’intérêt du fait de leurs propriétés physiques telles que la piézoélectricité, la ferroélectricité ou encore leur permittivité élevée. Ainsi, on cherche à les intégrer dans les micro- et nano-systèmes dans lesquels on les retrouve généralement sous forme de couche mince dans une configuration de type capacité plane. En particulier, l’oxyde de plomb, titane et zirconium (PZT) est un matériau très attractif pour les applications RF capacitives du fait de sa grande permittivité. Son intégration sur des électrodes métalliques, i.e. les lignes coplanaires constituant le guide d’onde, implique de maîtriser sa croissance en film mince. L’application d’une tension dans un dispositif RF actif impose également de contrôler les propriétés électriques : nature des courants de fuite et comportement ferroélectrique du PZT. Dans ce contexte, les couches minces de PZT sont déposées par ablation laser (PLD) sur un empilement La₀.₆₇Sr₀.₃₃MnO₃ (LSMO) / Pt (111) déposé sur un substrat monocristallin de saphir. La couche d’accroche conductrice LSMO est nécessaire afin d’éviter la formation d’une phase pyrochlore paraélectrique. Le contrôle de l’orientation cristalline de la couche de LSMO permet de contrôler la texturation de la couche de PZT. Les courants de fuite au travers de l’empilement Pt/PZT/LSMO/Pt ont ensuite été étudiés dans l’intervalle de température 220-330K de façon à déterminer les mécanismes de conduction. Une transition a été mise en évidence entre, autour de la température ambiante, un mécanisme contrôlé par la diffusion des charges en volume et, à basse température, un mécanisme contrôlé par l’injection des charges aux interfaces électrode/PZT. Un mécanisme par sauts a été identifié au-dessus de 280K en cohérence avec la présence de défauts étendus et la structure colonnaire du PZT. Afin de contrôler ces courants de fuite, différentes stratégies ont été utilisées. La première consiste à insérer une couche d’oxyde isolante à l’interface supérieure Pt/PZT modifiant ainsi l’injection des charges et permettant de réduire les courants de fuite. La seconde stratégie consiste, quant à elle, à modifier la structure de la couche de PZT en volume en élaborant des composites diélectrique/PZT multicouches ou colonnaires. Ainsi, une couche d’oxyde isolante a été insérée au milieu de la couche de PZT et a permis de réduire les courants de fuite. Le contrôle de la nucléation du PZT a également permis par nanofabrication d’élaborer un composite colonnaire pérovskite PZT/pyrochlore. La densité de piliers de pyrochlore dans la phase ferroélectrique permet de moduler la densité de courant dans la structure. Le PZT et les hétérostructures permettant de réduire les courants de fuite ont ensuite été intégrés dans une structure RF capacitive avec des lignes coplanaires d’or. Les performances RF en termes d’isolation et de pertes par insertion ainsi que la compatibilité de ces différents matériaux ont été étudiées et ont montré que les solutions développées dans le cadre du contrôle des courants de fuite sont prometteuses pour être intégrées dans les dispositifs RF capacitifs. En outre, on a cherché à extraire la permittivité à haute fréquence du PZT lorsque celui-ci est inséré dans une structure capacitive. Cette étude a notamment permis de mettre en évidence les points techniques à modifier concernant la structure du dispositif afin de parvenir à exploiter les propriétés physiques du PZT à haute fréquence. / Ferroelectric materials are raising a lot of interest due to their physical properties such as piezoelectricity, ferroelectricity or high dielectric constant. Thus, they are generally integrated in micro- and nano-systems as thin films in a capacitive configuration. Especially, the lead zirconate titanate oxide (PZT) is an attractive material for capacitive RF applications due to its high dielectric constant. The growth of the PZT thin film has to be controlled on metallic electrodes for its integration on coplanar transmission lines. Moreover, electrical properties such as leakage current and ferroelectric behavior of PZT have to be monitored upon application of a dc voltage bias for RF device operation. In this context, PZT thin films were grown by the pulsed laser deposition technique (PLD) on a La₀.₆₇Sr₀.₃₃MnO₃ (LSMO) / Pt (111) electrode on a monocrystalline sapphire substrate. The LSMO buffer layer is mandatory to avoid the formation of the paraelectric pyrochlore phase. The control of the crystalline orientation of the LSMO layer allows for the control of the PZT layer texture. Leakage currents through the Pt/PZT/LSMO/Pt stack were then studied in the 220-330K temperature range to determine the conduction mechanisms. A transition is evidenced between a bulk-controlled mechanism near room temperature and an interface-controlled mechanism at low temperature. A hopping mechanism is identified above 280K in line with the presence of extended defects and the columnar structure of the PZT layer. Several strategies were tested to control leakage currents. The first one consists in inserting an insulating oxide layer at the top Pt/PZT interface. In this way, charge injection was modified and leakage currents were reduced. The second strategy consists in changing the PZT layer bulk structure by elaborating a layered or columnar dielectric/PZT composite. Thus, an insulating oxide layer was inserted in the middle of the PZT layer and permitted to reduce leakage currents. Moreover, the control of the PZT nucleation allowed for the elaboration of a columnar PZT/pyrochlore composite. The leakage currents in this composite can be tuned through the pyrochlore pillars density among the ferroelectric matrix. Then, PZT and the heterostructures for leakage current control were integrated in a capacitive RF structure with gold coplanar transmission lines. RF performances in terms of isolation and insertion loss of these materials were studied and gave good results. In particular the heterostructures developed to control the leakage currents are promising for their integration in capacitive RF devices. Besides, I tried to extract the permittivity of PZT at high frequency with the PZT layer in a capacitive configuration. This study highlighted the essential modifications of the capacitive structure that have to be made in order to be able to exploit PZT properties at high frequency.

La miniaturisation toujours plus poussée des composants électroniques a atteint une limite en arrivant à l’échelle atomique. Afin de fabriquer des circuits à cette échelle, il est nécessaire de intéresser aux plus petits composants pouvant être intégrés : les molécules individuelles et les groupes d’atomes. Dans cette optique, les molécules de 1,4-bis(pyridin-4-ylethynyl) benzène (BPEB), Dibenzo[a,h]thianthrene (DBTH), de Bis{82,92,152,162,222,232- hexa-(2,4,6-trifluorophenoxy)[g,l,q]-5,10,15,20-tetraazaporphyrino)}[b,e]-benzene (H4Pc2) ont été conçues, synthétisées et caractérisées afin d’en étudier le transport de charges et les changements induits proche de la surface. Des techniques de SPM, tels que le STM, le nc-AFM et l’usage conjoint de l’AFM avec le STM ont été mises en pratique pour analyser les molécules reposant intégralement ou partiellement sur un substrat. L’interprétation des résultats expérimentaux a été faite au moyen de calculs de DFT. De plus, l’autoassemblage en solution de nouvelles mono-phthalocyanines métalliques fluorées, MPc (M= Mg2+, 2H+, Co2+) a été étudié.Tout d’abord, les mesures de conductance mirent en évidence, lors d’expériences de manipulation de fils moléculaires (BEPB), les changements de conformation associés aux transport des électrons à travers les molécules. De plus, le mouvement dit de “retournement papillon” (anglais: butterfly flapping) ayant lieu dans la classe des thianthrènes fut bloqué à basse température grâce à l’interaction avec le substrat. Ce blocage a permit de conduire la première étude stéréochimique de dérivés de thianthrènes chiraux (DBTH). Les analyses STM du DBTH ont montrées que le passage entre deux configurations de DBTH est reproductible et non-destructif. Par ailleurs, le nc-AFM utilisé à résolution sub-moléculaire a constitué un outils important pour réaliser une caractérisation complète et distinguer entre les différents isomères de configuration et de constitution déposés sur une surface. D’autre part, la structure moléculaire de la phthalocyanine binucléaire (H4Pc2) a été confirmée en utilisant un STM en mode “courant constant” et un AFM en mode “fréquence constante”. Ces résultats jettent les bases d’une prochaine étude de transport (travail en cours). En outre, l’étude de l’agrégation dans les molécules de MPc mit en évidence le rôle important de la capacité de coordination de l’atome central de la cavité Pc sur la formation d’agrégat. Finalement, des mesures électrochimiques ont démontrées que l’agrégation moléculaire peut bloquer le nature active de l’atome Co2+. Dans ce travail, il a été clairement montré que le SPM est une technique adéquate pour étudier les changements de conformations et de configurations associés aux courant tunnel d’électrons à travers des molécules, qu’elles soient planaire ou pas. Les études d’agrégation des interrupteurs magnétiques ont permis de mieux comprendre l’organisation supramoléculaire. Cette organisation est un point crucial pour le développement de futurs circuits basés sur une fabrication “bottom-up”. / The demand of downscaling of technology will reach its limit at the atomic length scale. This claim creates the necessity of investigating the smallest components suitable to become devices, single molecules or group of atoms. Therefore, 1,4-bis(pyridin-4-ylethynyl) benzene (BPEB), Dibenzo[a,h]thianthrene (DBTH) and Bis{82,92,152,162,222,232-hexa-(2,4,6-trifluorophenoxy)[g,l,q]-5,10,15,20-tetraazaporphyrino)}[b,e]-benzene (H4Pc2) have been designed, synthesized and characterized to investigate transport of charge through molecules and surface confined molecular switching. Scanning Probe Microscopy (SPM), such as STM, nc-AFM and combined STM/AFM were used to study the molecules on near-surface conditions. Density Functional Theory (DFT) calculations were used to interpret the experimental results. Moreover, the self-assembly of new fluorinated metalo mono-phthalocyanines, MPc (M= Mg2+, 2H+, Co2+) was investigated in solution.Firstly, conductance experiments performed while a molecular wire (BPEB) was being lifted up from a surface revealed the conformational changes associated to the transport of electrons through molecules. Secondly, the “butterfly” flapping motion in the class of the thianthrenes was blocked due to the interaction with a surface at low temperature. This block leads to the first stereochemical study of a quiral thianthere derivative (DBTH). The STM experiments on DBTH revealed a reproducible and non-destructive switching between two surface confined configurations of DBTH. In addition, nc-AFM with submolecular resolution has been proved to be a powerful tool for the full characterization and distinction of configurational and constitutional isomers on surfaces. Thirdly, the molecular structure of a binuclear phthalocyanine (H4Pc2) was confirmed through constant current STM and constant high _f AFM experiments. These results set the state of future spintronic transport experiments (ongoing work). On the other hand, the aggregation studies on MPc revealed that the coordination character of the central atom of the Pc cavity has an important effect on the formation of aggregates. Additionally, electrochemical experiments demonstrated that molecular aggregations can lead to the quenching of the electrochemical-active nature of a Co2+ atom.Herein it has been demonstrated that SPM are suitable techniques to study the conformational and configurational changes associated with the tunneling of electrons through planar and non-planar molecules in real space. Aggregation studies of magnetic switches were carried out to better understand the supramolecular organization under near surface conditions, a key point for the design of future devices based on the bottom up approach.

The aim of the diploma thesis is the reconstruction of Prostějov hl. n. railway station. The platforms with access persons with reduced mobility are designed in this station. The rail substructure and station drainage system design was necessary to do within the reconstruction. New assembly of a switches and crossing is the part of reconstruction design as well.

Kapazitive Sensoren, insbesondere kapazitive Näherungsschalter, werden aufgrund ihrer Fähigkeit nahezu beliebige Materialien detektieren zu können bereits seit vielen Jahrzehnten in unterschiedlichsten Applikationen der industriellen Messtechnik eingesetzt. Aufgrund ihrer kompakten Bauform, ihrer hohen Robustheit und ihres vergleichsweise günstigen Preises werden diese Sensoren auch heute noch in vielen Anwendungen eingesetzt. Wegen ihrer hohen Empfindlichkeit auf jegliche Änderung der elektrischen Eigenschaften in der Umgebung der Messelektrode werden kapazitive Näherungsschalter bei der berührungslosen Erkennung von Grenzständen eingesetzt, wobei der Sensor an der Außenseite eines nicht-leitenden Behälters angebracht ist. In den letzten Jahren sind die Anforderungen an die Sensorik immer weiter gestiegen. Statt einfacher Näherungsschalter, die ein binäres Schaltsignal ausgeben, werden heute zunehmend Sensoren gefordert, die ähnlich kompakt sind und die Sensorkapazität als Prozesswert ausgeben. Dadurch können potenziell neue Anwendungsfelder erschlossen werden. Insbesondere bei der Erkennung hoch-leitfähiger Medien sind Anhaftungen, die sich im Bereich der Messelektrode auf der Behälterinnenseite absetzen, problematisch. Die von den Sensoren gemessene Kapazität ist für das Vorhandensein einer leitfähigen Anhaftung und den tatsächlichen Vollzustand nahezu identisch, was zu Fehlauslösungen des Sensors führen kann. Es existieren bereits Ansätze leitfähige Anhaftungen auszublenden, wie beispielsweise die Verwendung kurzer Impulse als Anregungssignal. Allerdings sind die bei diesen Verfahren auftretenden großen Messfrequenzen ungünstig für das Sensorverhalten bezüglich der elektromagnetischen Verträglichkeit. Weiterhin können alternative Messprinzipien, wie beispielsweise Wirbelstromverfahren, verwendet werden. Bei diesen Verfahren ist jedoch die minimale Leitfähigkeit des Mediums, das detektiert werden kann, begrenzt. Ziel dieser Arbeit ist die Entwicklung eines Verfahrens zur Anhaftungserkennung bei kapazitiven Näherungsschaltern, das zusätzlich Informationen über das zu detektierende Medium liefert. Mit Hilfe der Impedanzspektroskopie gekoppelt mit analytischen und numerischen Modellierungsverfahren wird ein aus drei Parametern bestehendes vereinfachtes Modell entwickelt, das die zuverlässige Unterscheidung von Voll- Leer- und Anhaftungszustand ermöglicht. Einer dieser Parameter, der Gesamtwiderstand, erlaubt Rückschlüsse auf die Leitfähigkeit des zu detektierenden Mediums. Dieses neue Verfahren hat das Potenzial auch in komplexeren Applikationen Anwendung zu finden. / Capacitive sensors, especially capacitive proximity switches, are used in many applications because of their ability to detect almost any material. These sensors are still commonly used today due to their compact design, their high robustness and their comparatively low price. Because of their high sensitivity to changes of the electrical properties of materials in vicinity of the measurement electrode, capacitive proximity switches can be used for contactless limit level sensing. The sensor is often mounted on the outside of the liquid container. In recent years, requirements in regard to sensor performance have increased. Instead of just outputting a binary signal, capacitive proximity switches are expected to also output their measured capacitance, which could potentially open new fields of application. When detecting highly conductive fluids, soiling on the inside of the container in vicinity of the measurement electrode is problematic. The measured capacitance of a conductive film and the actual limit level are almost identical, which can cause false positive detection of a limit level. There are already various approaches to compensate for conductive soiling in vicinity of the measurement electrode, one of which includes the usage of short impulses for excitation. However, the high frequencies involved in these methods can cause problems with respect to electromagnetic compatibility. In addition, alternative measurement principles, like the eddy current principle, can be used. However, this principle imposes constraints on the minimum conductivity of the material to be detected. In this work, a technique to distinguish between conductive soiling and the actual fill level, which also allows to extract information about the material to be detected, is developed. Using impedance spectroscopy combined with analytical and numerical modelling, a model consisting of three parameters is developed. The model allows to reliably distinguish between actual limit level and conductive soiling. The overall resistance supplied by the model can be used as a measure for the conductivity of the material to be detected. The technique has the potential to be used in demanding applications.

The goal of this thesis was to design the reconstruction of the railway station Svitavy. The line speed was rised from the current value to 160 km·h-1. New platforms were designed, therefore the railway substructure and the drainage were adjusted accordingly. Also, the effective length of the main tracks was extended to 740 m.

Characterizing  power  switches  is  an  indispensable  step  when  designing  a  converter.  This  thesisinvestigates ways to achieve static and dynamic characterization of semiconductors for high power applications such as power grid or train traction. The static characterization has been tested with a Keysight B1506A device analyzer. The problems encountered have been analyzed and corrected.Then the design of a high current switching test bench for dynamic characterization is explained. The full-bridge  configuration  allows  controlled  and  spontaneous  commutations  so  the  bench  can measure hard and soft switching. The voltage can be up to 10 kV and the current up to 3 kA during the commutation. The choice of the probes is justified. The issues of bandwidth, input impedance and common mode current are taken into account. Data are processed in order to interpolate theswitching loss in hard and soft switching. / Karaktärisering  av  halvledarbrytare  är  ett  viktigt  steg  när  man  utformar  en  omvandlare.  Dennaavhandling undersöker olika sätt att uppnå statisk och dynamisk karakterisering av halvledare för högeffekttillämpningar såsom elnät eller ellok. Statisk karaktäriseringen har utförts med en Keysight B1506A-enhetsanalysator. De problem som uppstått har analyserats och korrigerats.Utformningen    av    en    testbänk    för    dynamisk    karakterisering    förklaras.    Den    kompletta bryggkonfigurationen möjliggör kontrollerad och spontan kommutation med spänningar upp till 10 kV och  strömmar  upp till 3 kA så att  bänken kan mäta hård  och mjuk  växling.  Valet  av sonderna förklaras.   Frågorna   om   bandbredd,   ingångsimpedans   och   common-mode   ström   tas   med   iberäkningen. Data bearbetas för att interpolera kopplings förlusten i hård och mjuk växling.

Tesis por compendio / [ES] La fotónica de silicio es una tecnología emergente clave en redes de comunicación e interconexiones de centros de datos de nueva generación, entre otros. Su éxito se basa en la utilización de plataformas compatibles con la tecnología CMOS para la integración de circuitos ópticos en dispositivos pequeños para una producción a gran escala a bajo coste. Dentro de este campo, los interferómetros integrados juegan un papel crucial en el desarrollo de diversas aplicaciones fotónicas en un chip como sensores biológicos, moduladores electro-ópticos, conmutadores totalmente ópticos, circuitos programables o sistemas LiDAR, entre otros. Sin embargo, es bien sabido que la interferometría óptica suele requerir caminos de interacción muy largos, lo que dificulta su integración en espacios muy compactos. Para mitigar algunas de estas limitaciones de tamaño, surgieron varios enfoques, incluyendo materiales sofisticados o estructuras más complejas, que, en principio, redujeron el área de diseño pero a expensas de aumentar los pasos del proceso de fabricación y el coste. Esta tesis tiene como objetivo proporcionar soluciones generales al problema de tamaño típico de los interferómetros ópticos integrados, con el fin de permitir la integración densa de dispositivos basados en silicio. Para ello, aunamos los beneficios tanto de las guías de onda bimodales como de las estructuras periódicas, en términos de la mejora del rendimiento y la posibilidad para diseñar interferómetros monocanal en áreas muy reducidas. Más específicamente, investigamos los efectos dispersivos que aparecen en estructuras menores a la longitud de onda y en las de cristal fotónico, para su implementación en diferentes configuraciones interferométricas bimodales. Además, demostramos varias aplicaciones potenciales como sensores, moduladores y conmutadores en tamaños ultra compactos de unas pocas micras cuadradas. En general, esta tesis propone un nuevo concepto de interferómetro integrado que aborda los requisitos de tamaño de la fotónica actual y abre nuevas vías para futuros dispositivos basados en funcionamiento bimodal. / [CA] La fotònica de silici és una tecnologia emergent clau en xarxes de comunicació i interconnexions de centres de dades de nova generació, entre altres. El seu èxit es basa en la utilització de plataformes compatibles amb la tecnologia CMOS per a la integració de circuits òptics en dispositius diminuts per a una producció a gran escala a baix cost. Dins d'aquest camp, els interferòmetres integrats juguen un paper crucial en el desenvolupament de diverses aplicacions fotòniques en un xip com a sensors biològics, moduladors electro-òptics, commutadors totalment òptics, circuits programables o sistemes LiDAR, entre altres. No obstant això, és ben sabut que la interferometría òptica sol requerir camins d'interacció molt llargs, la qual cosa dificulta la seua integració en espais molt compactes. Per a mitigar algunes d'aquestes limitacions de grandària, van sorgir diversos enfocaments, incloent materials sofisticats o estructures més complexes, que, en principi, van reduir l'àrea de disseny però a costa d'augmentar els processos de fabricació i el cost. Aquesta tesi té com a objectiu proporcionar solucions generals al problema de grandària típica dels interferòmetres òptics integrats, amb la finalitat de permetre la integració densa de dispositius basats en silici. Per a això, combinem els beneficis tant de les guies d'ones bimodals com de les estructures periòdiques, en termes de funcionament d'alt rendiment per a dissenyar interferòmetres monocanal compactes en àrees molt reduïdes. Més específicament, investiguem els efectes dispersius que apareixen en estructures menors a la longitud d'ona i en les de cristall fotònic, per a la seua implementació en diferents configuracions interferomètriques bimodals. A més, vam demostrar diverses aplicacions potencials com a sensors, moduladors i commutadors en grandàries ultres compactes d'unes poques micres cuadrades. En general, aquesta tesi proposa un nou concepte d'interferòmetre integrat que aborda els requisits de grandària de la fotònica actual i obri noves vies per a futurs dispositius basats en funcionament bimodal. / [EN] Silicon photonics is a key emerging technology in next-generation communication networks and data centers interconnects, among others. Its success relies on the ability of using CMOS-compatible platforms for the integration of optical circuits into small devices for a large-scale production at low-cost. Within this field, integrated interferometers play a crucial role in the development of several on-chip photonic applications such as biological sensors, electro-optic modulators, all-optical switches, programmable circuits or LiDAR systems, among others. However, it is well known that optical interferometry usually requires very long interaction paths, which hinders its integration in highly compact footprints. To mitigate some of these size limitations, several approaches emerged including sophisticated materials or more complex structures, which, in principle, reduced the design area but at the expense of increasing fabrication process steps and cost. This thesis aims at providing general solutions to the long-standing size problem typical of optical integrated interferometers, in order to enable the densely integration of silicon-based devices. To this end, we combine the benefits from both bimodal waveguides and periodic structures, in terms of high-performance operation and compactness to design single-channel interferometers in very reduced areas. More specifically, we investigate the dispersive effects that arise from subwavelength grating and photonic crystal structures for their implementation in different bimodal interferometric configurations. Furthermore, we demonstrate various potential applications such as sensors, modulators and switches in ultra-compact footprints of a few square microns. In general, this thesis proposes a new concept of integrated interferometer that addresses the size requirements of current photonics and open up new avenues for future bimodal-operation-based devices. / Financial support is also gratefully acknowledged through postdoctoral FPI grants from Universitat Politècnica de València (PAID-01-18). European Commission through the Horizon 2020 Programme (PHC-634013 PHOCNOSIS project). The authors acknowledge funding from the Generalitat Valenciana through the AVANTI/2019/123, ACIF/2019/009 and PPC/2020/037 grants and from the European Union through the operational program of the European Regional Development Fund (FEDER) of the Valencia Regional Government 2014–2020. / Torrijos Morán, L. (2021). Photonic Applications Based on Bimodal Interferometry in Periodic Integrated Waveguides [Tesis doctoral]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/172163 / Compendio

No contexto da operação de sistemas de distribuição, um dos problemas com os quais os operadores lidam frequentemente é o de restabelecimento de energia. Este problema surge na ocorrência de uma falta permanente e pode ser tratado por meio de manobras em chaves presentes na rede primária. Uma vez que tais redes operam com topologia radial, a ocorrência de uma falta pode resultar no desligamento de consumidores saudáveis. Desta maneira, o problema consiste em definir, num curto intervalo de tempo, um número mínimo de chaves que devem ser operadas a fim de isolar a falta e restaurar o máximo de consumidores saudáveis desligados. Os esforços para a obtenção de ferramentas computacionais para fornecimento de soluções para o problema de restabelecimento têm sido intensificados nos últimos anos. Isto ocorre, em especial, devido aos enormes prejuízos causados pela falta de energia às companhias de eletricidade e a toda a sociedade. Neste sentido, o objetivo deste trabalho é a obtenção de um método para auxiliar o trabalho dos operadores através do fornecimento de planos adequados de restabelecimento em curtos intervalos de tempo. Os diferenciais deste método proposto são a sua capacidade de: lidar, em especial, com redes reais de grande porte com reduzido esforço computacional; considerar a existência de vários níveis de prioridade de atendimento entre os consumidores (note, por exemplo, que um hospital ou um centro de segurança pública devem ter maior prioridade de atendimento que um grande supermercado ou unidades residenciais) e priorizar o atendimento deles de acordo a sua prioridade; fornecer uma sequência por meio da qual as chaves possam ser operadas a fim de isolar os setores em falta e reconectar o maior número de consumidores saudáveis desligados executando-se o mínimo de manobras em chaves e priorizando os consumidores com maior prioridade; ser capaz de selecionar cargas menos prioritárias para permaneceram desligadas nas situações em que não é possível obter uma solução que restaure todas as cargas saudáveis fora de serviço; e, adicionalmente, priorizar a operação de chaves controladas remotamente, que, diferentemente das chaves controladas manualmente, podem ser operadas com menores custos e de maneira mais rápida. O método proposto consiste, de maneira sintética, na união de uma busca exaustiva aplicada localmente a um novo algoritmo evolutivo multi-objetivo em tabelas de subpopulação que faz uso de uma estrutura de dados eficiente denominada Representação Nó-Profundidade. Para avaliar a performance relativa do método proposto, simulações foram realizadas num sistema de distribuição de pequeno porte e os resultados foram comparados com os obtidos por um método de Programação Matemática. Na sequência, novos experimentos foram realizadas em diversos casos de falta na rede de distribuição da cidade de Londrina-PR e cidades adjacentes. As soluções fornecidas mostraram-se adequadas ao tratamento dos casos de falta, assim como as sequências de chaveamento associadas a elas, as quais foram capazes de priorizar o restabelecimento dos consumidores prioritários seguindo seus níveis de prioridade. Adicionalmente, estudos avaliaram a variação do tempo de processamento computacional do método proposto com a dimensão das redes de distribuições e também com o número de gerações realizadas pelo algoritmo evolutivo multi-objetivo proposto e os resultados mostraram-se satisfatórios às necessidades do problema Portanto, pode-se comprovar que o método proposto atingiu os objetivos especificados, em especial, o tratamento de aspectos práticos do problema. Além do próprio método proposto, algumas contribuições desta pesquisa são a proposição um novo algoritmo evolutivo multiobjetivo em tabelas de subpopulação e de um novo operador para manipulação de florestas de grafo armazenadas pela Representação Nó-Profundidade e voltado ao problema de restabelecimento. / In the context of distribution systems operation, service restoration is one of the problems with which operators constantly deal. It arises when a permanent fault occurs and is treated trough operations in switches at primary grid. Since distribution systems are usually radial, fault occurrence turns-off healthy customers. Thereby, the service restoration problem consists in defining, in a short processing time, the minimum amount of switches that must be operated for the isolation of the fault and reconnection of the maximum amount of healthy out-of-service customers. The efforts of developing computational tools for getting solution to this problems has increased in the last years. It is, in special, due to enormous losses caused to the utilities and to the whole society. In this sense, the main objective of this research is getting a method able to help the distribution system operator\'s work through providing service restoration plans quickly. The differentials of this research are its ability to: deal, in special, with large scale grids whit a reduced computational effort; consider costumers of several priority levels (note, for instance, a hospital has a higher supply priority in relation to a big supermarket) and prioritize the higher priority customers; provide a switching sequence able to isolate and reconnect the maximum amount of healthy out-of-service customer by the minimum amount of switching actions; select lower priority customers to keep out-of-service in order to reconnect higher priority customers when a it is not possible to restore all customers; and, additionally, prioritize switching operation in remotely controlled switches, whose operation is faster and cheapest than the operation of manually controlled switches. The proposed method mixes a local exhaustive search and a new multi-objective evolutionary algorithm in subpopulation tables that uses a data structure named Node-Depth Encoding. For evaluating the relative performance of proposed method, simulations were performed in small distribution systems and the performance was compared with the performance a Mathematical Programing method from literature. New experiments were performed a Mathematical Programing method from literature. New experiments were performed in several fault situations in the real and large-scale distribution system of Londrina-PR and adjacent cities. The solutions provided were appropriated to the treatment of such contingency situations. The same occurs with the switching sequences provided, which were able to prioritize the restoration of higher priority customers. Additional studies evaluated the variation of the running time with the size of grids and with the values adopted for the maximum number of generations of the evolutionary algorithm (which is an input parameter). The results expressed the running time of the proposed method is suitable to the problem needs. Therefore, it could be proved the proposed method achieved the specified objectives, in special, the treatment of practical aspects of the problem. Besides the proposed method, some contributions of this research are proposition of a new multi-objective evolutionary algorithm in subpopulation tables and a new reproduction operator to manipulate graph forests computationally represented by Node-Depth Encoding.

Ce manuscrit est une contribution à l’étude de la fiabilité et de la robustesse des composants MOSFET sur carbure de silicium, matériau semi-conducteur grand gap qui possède des caractéristiques bien meilleures que le silicium. Ces nouveaux interrupteurs de puissances permettent d’obtenir entre autres propriétés remarquables, des fréquences de commutations et des tenues en tension plus élevées dans les systèmes de conversions de puissance. Ils sont particulièrement mis en avant depuis un peu plus d’une dizaine d’années pour les gains en performances, diminution des tailles et poids qu’ils apportent à certaines topologies de convertisseurs pour les réseaux haute tension à courant continu. Puis sont répertoriés les principaux mécanismes de défaillances de ces MOSFET SiC induits par la faiblesse de la grille. Toutes les mesures nécessaires au suivi des paramètres clés lors des prochains vieillissements sont présentées. Les résultats de nos tests sur l’instabilité de la tension de seuil sont aussi détaillés et un modèle empirique pour valider le comportement de relaxation observé est proposé. Celui-ci nous aidera par la suite à établir un protocole de mesure rigoureux de la tension de seuil. Les tests expérimentaux et résultats de vieillissement en statique et dynamique sur les composants 1,7 kV vont permettre de se rendre compte de l’importance de la dérive de la tension de seuil sur 1000 h. Dans le cas d’un vieillissement statique, il y a environ 7 % de dérive positive du VTH et un pourcentage équivalent pour les tests dynamiques. Des analyses supplémentaires (C-V et pompage de charge) sur l’oxyde de grille en cours de vieillissement sont proposées pour une meilleure compréhension des mécanismes mis en jeu dans la dégradation de l’oxyde. Enfin, les derniers tests présentés seront focalisés sur le comportement en court-circuit et courts-circuits répétitifs des mêmes composants. Avec une énergie critique évaluée autour de 1,5 J nos tests sur les MOSFET 1,7 kV montrent les limites de la robustesse de ces composants, avec une tenue en court-circuit bien inférieure à 10 µs et une incapacité à résister à plus de 150 courts-circuits successifs. L’influence de la tension entre drain et source y est notamment étudiée, et montre que l’énergie critique supportée par le composant diminue avec l’augmentation de cette tension. / This manuscript is a contribution to reliability and robustness study of MOSFET components on silicon carbide “SiC”, wide band gap semiconductor with better characteristics compared to silicon “Si” material. Those new power switches can provide better switching frequencies or voltage withstanding for example in power converter. SiC MOSFET are the results of approximately 10 years of research and development and can provide increased performances and weight to some converter topology for high voltage direct current networks. Others power switches available are still introduced and an introduction to reliability is explaining why such work on this new power switches is important. Transition from Si technologies to SiC ones require a lot of work regarding its robustness. Before showing reliability and robustness results is presented I give a lot of details regarding to the measurement and monitoring of key parameters used in the next chapters. The results of our tests on the threshold voltage instability are presented and how we validated an empirical model on this drift. This was used to propose an enhanced measurement protocol on the threshold voltage. Static and dynamic experimental results presented next will show if the voltage drift during ageing is significant or not. Further analysis is proposed to add more insight on the understanding of the oxide degradation mechanisms through C-V and charge pumping measurements. Finally, the ageing results presented on 1,7 kV SiC MOSFET are focused on the short-circuit and repetitive short-circuit behavior of the same components. Drain to source voltage influence on critical energy during this particular and stressful operation mode is studied. This time, the results are worrying.The last chapter is confidential.

No contexto da operação de sistemas de distribuição, um dos problemas com os quais os operadores lidam frequentemente é o de restabelecimento de energia. Este problema surge na ocorrência de uma falta permanente e pode ser tratado por meio de manobras em chaves presentes na rede primária. Uma vez que tais redes operam com topologia radial, a ocorrência de uma falta pode resultar no desligamento de consumidores saudáveis. Desta maneira, o problema consiste em definir, num curto intervalo de tempo, um número mínimo de chaves que devem ser operadas a fim de isolar a falta e restaurar o máximo de consumidores saudáveis desligados. Os esforços para a obtenção de ferramentas computacionais para fornecimento de soluções para o problema de restabelecimento têm sido intensificados nos últimos anos. Isto ocorre, em especial, devido aos enormes prejuízos causados pela falta de energia às companhias de eletricidade e a toda a sociedade. Neste sentido, o objetivo deste trabalho é a obtenção de um método para auxiliar o trabalho dos operadores através do fornecimento de planos adequados de restabelecimento em curtos intervalos de tempo. Os diferenciais deste método proposto são a sua capacidade de: lidar, em especial, com redes reais de grande porte com reduzido esforço computacional; considerar a existência de vários níveis de prioridade de atendimento entre os consumidores (note, por exemplo, que um hospital ou um centro de segurança pública devem ter maior prioridade de atendimento que um grande supermercado ou unidades residenciais) e priorizar o atendimento deles de acordo a sua prioridade; fornecer uma sequência por meio da qual as chaves possam ser operadas a fim de isolar os setores em falta e reconectar o maior número de consumidores saudáveis desligados executando-se o mínimo de manobras em chaves e priorizando os consumidores com maior prioridade; ser capaz de selecionar cargas menos prioritárias para permaneceram desligadas nas situações em que não é possível obter uma solução que restaure todas as cargas saudáveis fora de serviço; e, adicionalmente, priorizar a operação de chaves controladas remotamente, que, diferentemente das chaves controladas manualmente, podem ser operadas com menores custos e de maneira mais rápida. O método proposto consiste, de maneira sintética, na união de uma busca exaustiva aplicada localmente a um novo algoritmo evolutivo multi-objetivo em tabelas de subpopulação que faz uso de uma estrutura de dados eficiente denominada Representação Nó-Profundidade. Para avaliar a performance relativa do método proposto, simulações foram realizadas num sistema de distribuição de pequeno porte e os resultados foram comparados com os obtidos por um método de Programação Matemática. Na sequência, novos experimentos foram realizadas em diversos casos de falta na rede de distribuição da cidade de Londrina-PR e cidades adjacentes. As soluções fornecidas mostraram-se adequadas ao tratamento dos casos de falta, assim como as sequências de chaveamento associadas a elas, as quais foram capazes de priorizar o restabelecimento dos consumidores prioritários seguindo seus níveis de prioridade. Adicionalmente, estudos avaliaram a variação do tempo de processamento computacional do método proposto com a dimensão das redes de distribuições e também com o número de gerações realizadas pelo algoritmo evolutivo multi-objetivo proposto e os resultados mostraram-se satisfatórios às necessidades do problema Portanto, pode-se comprovar que o método proposto atingiu os objetivos especificados, em especial, o tratamento de aspectos práticos do problema. Além do próprio método proposto, algumas contribuições desta pesquisa são a proposição um novo algoritmo evolutivo multiobjetivo em tabelas de subpopulação e de um novo operador para manipulação de florestas de grafo armazenadas pela Representação Nó-Profundidade e voltado ao problema de restabelecimento. / In the context of distribution systems operation, service restoration is one of the problems with which operators constantly deal. It arises when a permanent fault occurs and is treated trough operations in switches at primary grid. Since distribution systems are usually radial, fault occurrence turns-off healthy customers. Thereby, the service restoration problem consists in defining, in a short processing time, the minimum amount of switches that must be operated for the isolation of the fault and reconnection of the maximum amount of healthy out-of-service customers. The efforts of developing computational tools for getting solution to this problems has increased in the last years. It is, in special, due to enormous losses caused to the utilities and to the whole society. In this sense, the main objective of this research is getting a method able to help the distribution system operator\'s work through providing service restoration plans quickly. The differentials of this research are its ability to: deal, in special, with large scale grids whit a reduced computational effort; consider costumers of several priority levels (note, for instance, a hospital has a higher supply priority in relation to a big supermarket) and prioritize the higher priority customers; provide a switching sequence able to isolate and reconnect the maximum amount of healthy out-of-service customer by the minimum amount of switching actions; select lower priority customers to keep out-of-service in order to reconnect higher priority customers when a it is not possible to restore all customers; and, additionally, prioritize switching operation in remotely controlled switches, whose operation is faster and cheapest than the operation of manually controlled switches. The proposed method mixes a local exhaustive search and a new multi-objective evolutionary algorithm in subpopulation tables that uses a data structure named Node-Depth Encoding. For evaluating the relative performance of proposed method, simulations were performed in small distribution systems and the performance was compared with the performance a Mathematical Programing method from literature. New experiments were performed a Mathematical Programing method from literature. New experiments were performed in several fault situations in the real and large-scale distribution system of Londrina-PR and adjacent cities. The solutions provided were appropriated to the treatment of such contingency situations. The same occurs with the switching sequences provided, which were able to prioritize the restoration of higher priority customers. Additional studies evaluated the variation of the running time with the size of grids and with the values adopted for the maximum number of generations of the evolutionary algorithm (which is an input parameter). The results expressed the running time of the proposed method is suitable to the problem needs. Therefore, it could be proved the proposed method achieved the specified objectives, in special, the treatment of practical aspects of the problem. Besides the proposed method, some contributions of this research are proposition of a new multi-objective evolutionary algorithm in subpopulation tables and a new reproduction operator to manipulate graph forests computationally represented by Node-Depth Encoding.