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The use of Silicon Carbide Field Effect Transistor (SiC-FET) sensors in cyclic operation is a proven way to quantify different gases. The standard workflow involves extracting shape-defining features such as averages and slopes of the sensor signal. This work’s main goal is to verify if frequency modulation can be used to simultaneously quantify Nitric Oxide (NO), Nitrogen Dioxide (NO2) and Ammonia (NH3). Linear models were chosen, namely: Ordinary Least Squares (OLS), Principal Components Regression (PCR), Partial Least Squares Regression (PLSR) and Ridge regression. Results indicate that these models fail to predict concentrations completely for every gas. Analysis indicates that the features are not linear in terms of concentrations. This work is concluded by recommending a few other alternatives before discarding frequency cycling completely: non-parametric models of regression and different frequency regime, namely the use of triangular waves in future experiments.

<p>Light emitting diode (LED)-based solid state displays (SSD) have attracted growing interest due to their advantages in terms of contrast ratio, brightness, viewing angle, and response time compared to liquid crystal displays. GaN based III-nitride thin film materials are suitable materials for SSD due to their wide and tunable bandgaps. However, the large size and costly manufacturing process of commercially available GaN-based LED chips limit the potential uses of LEDs as the pixels of SSD.</p> <p>In this work, tiny single crystal beta-phase (111) oriented SiC whiskers 2 microns in diameter and 18 microns in length are proposed as the substrates for GaN growth due to their small lattice constant mismatch (3%) with GaN, their conductive nature and their small size for potential use in SSD pixels. Aligned SiC whiskers with (111) planes exposed in an alumina matrix prepared by a precise manipulation and alignment method of SiC whiskers including a series of steps was developed in this work. The alignment degree of whiskers achieved in this work is higher than conventional extrusion methods, and a sintering approach capable of forming an aligned alumina/SiC composite was developed and understood using a self-limiting oxidation reaction mechanism.</p> <p>To take advantage of the potential versatility, scalability and cost effectiveness of sputtering for SSD manufacturing, a reactive sputtering system was built for a detailed investigation of GaN thin film growth nucleation and subsequent growth behavior on SiC. 6H-SiC single crystal substrates were chosen as a reference substrate for SiC whiskers. An XRRC indicates that a high quality single crystalline GaN thin film was successfully grown epitaxially on 6H-SiC by sputtering. Two-dimensional X-ray diffraction and scanning transmission electron microscopy results demonstrated that the epitaxial growth of GaN thin films relies on the short range order and/or crystalline area of the native oxide layer in GaN/SiC interface for the first time.</p> / Doctor of Philosophy (PhD)

This dissertation introduces a hierarchical optimization framework for power converter-based energy management systems, with a primary focus on weight minimization. Emphasizing modularity and scalability, the research systematically tackles the challenges in optimizing these systems, addressing complex design variables, couplings, and the integration of heterogeneous models. The study begins with a comparative evaluation of various metaheuristic optimization methods applied to power inductors and converters, including genetic algorithm, particle swarm optimization, and simulated annealing. This is complemented by a global sensitivity analysis using the Morris method to understand the impact of different design variables on the design objectives and constraints in power electronics. Additionally, a thorough evaluation of different modeling methods for key components is conducted, leading to the validation of selected analytical models at the component level through extensive experiments. Further, the research progresses to studies at the converter level, focusing on a weight-optimized design for the thermal management systems for silicon carbide (SiC) MOSFET-based modular converters and the development of a hierarchical digital control system. This stage includes a thorough assessment of the accuracy of small-signal models for modular converters. At this point, the research methodically examines various design constraints, notably thermal considerations and transient responses. This examination is critical in understanding and addressing the specific challenges associated with converter-level design and the implications on system performance. The dissertation then presents a systematic approach where design variables and constraints are intricately managed across different hierarchies. This strategy facilitates the decoupling of subsystem designs within the same hierarchy, simplifying future enhancements to the optimization process. For example, component databases can be expanded effortlessly, and diverse topologies for converters and subsystems can be incorporated without the need to reconfigure the optimization framework. Another notable aspect of this research is the exploration of the scalability of the optimization architecture, demonstrated through design examples. This scalability is pivotal to the framework's effectiveness, enabling it to adapt and evolve alongside technological advancements and changing design requirements. Furthermore, this dissertation delves into the data transmission architecture within the hierarchical optimization framework. This architecture is not only critical for identifying optimal performance measures, but also for conveying detailed design information across all hierarchy levels, from individual components to entire systems. The interrelation between design specifications, constraints, and performance measures is illustrated through practical design examples, showcasing the framework's comprehensive approach. In summary, this dissertation contributes a novel, modular, and scalable hierarchical optimization architecture for the design of power converter-based energy management systems. It offers a comprehensive approach to managing complex design variables and constraints, paving the way for more efficient, adaptable, and cost-effective power system designs. / Doctor of Philosophy / This dissertation introduces an innovative approach to designing energy control systems, inspired by the creativity and adaptability of a Lego game. Central to this concept is a layered design methodology. The journey begins with power components, the fundamental 'Lego bricks'. Each piece is meticulously optimized for compactness, forming the robust foundation of the system. Like connecting individual Lego bricks into a module, these power components come together to form standardized power converters. These converters offer flexibility and scalability, similar to how numerous structures can be built from the same set of Lego pieces. The final layer involves assembling these power converters in order to construct comprehensive energy control systems. This mirrors the process of using Lego subassemblies to build larger, more intricate structures. At this system-level design, the standardized converters are integrated to optimize overall system performance. Key to this dissertation's methodology is an emphasis on modularity and scalability. It enables the creation of diverse energy control systems of varying sizes and functionalities from these fundamental units. The research delves into the intricacies of design variables and constraints, ensuring that each 'Lego piece' contributes optimally to the bigger picture. This includes exploring the scalability of the architecture, allowing it to evolve with technological advancements and design requirements, as well as examining data transmission within the system to ensure efficient data communication across all levels. In essence, this dissertation is about recognizing the potential in the smallest components and understanding their role in the grand scheme of the system. It is akin to playing a masterful game of Lego, where building something greater from small, well-designed parts leads to more efficient, adaptable, and cost-effective energy control system designs. This approach is particularly relevant for applications in transportation systems and renewable energy in remote locations, showcasing the universal applicability of this 'Lego game' to energy management.

The work in this dissertation presents the first attempt in the literature to propose the concept of "soft switch". The goal of "soft switch" is to develop a standard PWM switch cell with built-in adaptive soft switching capabilities. Just like a regular switch, only one PWM signal is needed to drive the soft switch under soft switching condition. The core technique in soft switch development is a built-in adaptive soft switching circuit with minimized circulation energy. The necessity of minimizing circulation energy is first analyzed. The design and implementation of a universal controller for implementation of variable timing control to minimize circulation energy is presented. The controller has been tested successfully with three different soft switching inverters for electric vehicles application in the Partnership for a New Generation Vehicles (PNGV) project. To simplify the control, several methods to achieve soft switching with fixed timing control are proposed by analyzing a family of zero-voltage switching converters. The driver based soft switch concept was originated from development of a base driver circuit for current driven bipolar junction transistor (BJT). A new insulated-gate-bipolar-transistor (IGBT) and power metal-oxide-semiconductor field-effect-transistor (MOSFET) gated transistor (IMGT) base drive structure was initially proposed for a high power SiC BJT. The proposed base drive method drives SiC BJTs in a way similar to a Darlington transistor. With some modification, a new base driver structure can adaptively achieve zero voltage turn-on for BJT at all load current range with one single gate. The proposed gate driver based soft switching method is verified by experimental test with both Si and SiC BJT. The idea is then broadened for "soft switch" implementation. The whole soft switched BJT (SSBJT) structure behaves like a voltage-driven soft switch. The new structure has potentially inherent soft transition property with reduced stress and switching loss. The basic concept of the current driven soft switch is then extended to a voltage-driven device such as IGBT and MOSFET. The key feature and requirement of the soft switch is outlined. A new coupled inductor based soft switching cell is proposed. The proposed zero-voltage-transition (ZVT) cell serves as a good candidate for the development of soft switch. The "Equivalent Inductor" and state plane based analysis method are used to simply the analysis of coupled inductor based zero-voltage switching scheme. With the proposed analysis method, the operational property of the ZVT cell can be identified without solving complicated differential equations. Detailed analysis and design is proposed for a 3kW boost converter example. With the proposed soft switch design, the boost converter can achieve up to 98.9% efficiency over a wide operation range with a single gate drive. A high power inverter with coupled inductor scheme is also designed with simple control compared to the earlier implementation. A family of soft-switching converters using the proposed "soft switch" cell can be developed by replacing the conventional PWM switch with the proposed soft switch. / Ph. D.

In recent years, the SiC power semiconductor has emerged as an attractive alternative that pushes the limitations of junction temperature, power rating, and switching frequency of Si devices. These advanced properties will lead converters to higher power density. However, the reliability of the SiC semiconductor is still under investigation, and at the same time, the standard Si device packages do not meet the requirement of high temperature operation. In order to take full advantage of SiC semiconductor devices, high density, high temperature device packaging needs to be developed. In this dissertation, a high temperature wirebond package for multi-chip phase-leg power module using SiC devices was designed, developed, fabricated and tested. The details of the material selection and thermo-mechanical reliability evaluation are described. High temperature power test shows that the presented package can perform well at the high junction temperature. In order to increase the power density, reduce the parasitic parameters, and enhance the electrical, thermo-mechanical performance over wirebond packages, planar package is utilized to better take advantages of SiC device. This dissertation proposed a novel package, in which the interconnections can be formed on small dimensional pads and enclosed pads that may baffle the regular solder based connection in other planar packages. Electrical and thermo-mechanical tests of the prototype module demonstrate the functionality and reliability of the presented planar packaging methodology. In this dissertation, together with the design example, the manual module layout design and automatic module layout design process are also presented. Furthermore, a systematic optimal design process and parametric study of the heatsink-fan cooling system by applying the analytical model is described. This dissertation also established a systematic testing procedure which can rapidly detect defects and reduce the risk in high temperature packaging testing. Finally, a wirebond module and a planar module are designed for 175 ºC junction temperature and 250 ºC junction temperatures. All the key concepts and ideas developed in this work are implemented in the prototype module development and then verified by the experimental results. / Ph. D.